2-(methoxymethyl)-5-methylphenacyl benzoate

Base Information

Chemical Name:2-(methoxymethyl)-5-methylphenacyl benzoate
CAS No.:915085-77-7
Molecular Formula:C₁₈H₁₈O₄
Molecular Weight:298.339
Hs Code.:

Synonyms:2-(methoxymethyl)-5-methylphenacyl benzoate

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Chemical Property of 2-(methoxymethyl)-5-methylphenacyl benzoate

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Technology Process of 2-(methoxymethyl)-5-methylphenacyl benzoate

There total 2 articles about 2-(methoxymethyl)-5-methylphenacyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 915085-41-5
2-(methoxymethyl)-5-methyl-α-chloroacetophenone

: 65-85-0,8013-63-6
benzoic acid

: 915085-77-7
2-(methoxymethyl)-5-methylphenacyl benzoate

Guidance literature:: With triethylamine; sodium iodide; In acetone; for 6.5h; Heating;
DOI:10.1021/jo061169j

Reference yield:

: 66521-22-0
2-(methoxymethyl)-5-methylacetophenone

: 915085-77-7
2-(methoxymethyl)-5-methylphenacyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / SO₂Cl₂ / CH₂Cl₂ / 0.5 h / 20 °C

2: 69 percent / triethylamine; NaI / acetone / 6.5 h / Heating

With sulfuryl dichloride; triethylamine; sodium iodide; In dichloromethane; acetone;
DOI:10.1021/jo061169j

Reference yield:

: 915085-77-7
2-(methoxymethyl)-5-methylphenacyl benzoate

: 915085-73-3
2-acetyl-4-methyl-benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: NaHCO₃; H₂O / hexane / UV-irradiation

2: 42 percent / SO₂Cl₂ / CH₂Cl₂ / 0.5 h / 20 °C

3: H₂O; NaHCO₃ / hexane / 12 h / UV-irradiation

With sulfuryl dichloride; water; sodium hydrogencarbonate; In hexane; dichloromethane;
DOI:10.1021/jo061169j