{1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethoxy}acetic acid tert-butylester

Base Information

Chemical Name:{1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethoxy}acetic acid tert-butylester
CAS No.:916525-68-3
Molecular Formula:C₃₄H₄₆O₇
Molecular Weight:566.735
Hs Code.:

Synonyms:{1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethoxy}acetic acid tert-butylester

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Chemical Property of {1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethoxy}acetic acid tert-butylester

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Technology Process of {1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethoxy}acetic acid tert-butylester

There total 4 articles about {1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethoxy}acetic acid tert-butylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 916525-59-2
1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethanol

: 5292-43-3
bromoacetic acid tert-butyl ester

: 916525-68-3
{1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethoxy}acetic acid tert-butylester

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride; In tetrahydrofuran; for 12h; Heating;
DOI:10.1016/j.tetasy.2006.08.017

Reference yield:

: 6706-96-3
2,2'-dimethoxybenzoin

: 916525-68-3
{1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethoxy}acetic acid tert-butylester

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / sodium borohydride / ethanol / 0 - 20 °C

2: 70 percent / 4-methylbenzenesulfonic acid monohydrate / CH₂Cl₂ / 2 h / 20 °C

3: 72 percent / NaH; HMPT / tetrahydrofuran / 12 h / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; p-toluenesulfonic acid monohydrate; sodium hydride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/j.tetasy.2006.08.017

Reference yield:

: 61080-15-7
meso-1,2-bis(2-methoxyphenyl)ethane-1,2-diol

: 916525-68-3
{1,2-bis(2-methoxyphenyl)-2-[(7,8,8-trimethyloctahydro-4,7-methanobenzo[b]furan-2-yl)oxy]ethoxy}acetic acid tert-butylester

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 4-methylbenzenesulfonic acid monohydrate / CH₂Cl₂ / 2 h / 20 °C

2: 72 percent / NaH; HMPT / tetrahydrofuran / 12 h / Heating

With N,N,N,N,N,N-hexamethylphosphoric triamide; p-toluenesulfonic acid monohydrate; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetasy.2006.08.017