*)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride

Base Information

Chemical Name:*)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride
CAS No.:81602-13-3
Molecular Formula:C₁₉H₂₄N₂O₃*ClH
Molecular Weight:364.872
Hs Code.:

<S-(R<sup>*</sup>)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride

Synonyms:*)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride

Suppliers and Price of *)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of *)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride

Chemical Property:

Purity/Quality:: 95%+ or 98%+ ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of *)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride

There total 13 articles about *)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 81580-37-2
*,S^*)>-5-<1-hydroxy-2-ethyl>-2-(phenylmethoxy)benzamide

: 81602-13-3
*)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium dihydroxide; In ethanol; for 2h; under 2280 Torr; Ambient temperature;
DOI:10.1021/jm00353a017

Reference yield:

: 68164-04-5
N-benzyl-1-methyl-3-phenylpropylamine

: 81602-13-3
*)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

2: K₂CO₃ / dimethylformamide / 4 h / Ambient temperature

3: NaBH₄ / ethanol / 16 h / Ambient temperature

4: 70 percent / H₂, 1 N aq. HCl / 20percent Pd(OH)2/C / ethanol / 2 h / 2280 Torr / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; hydrogen; potassium carbonate; palladium dihydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00353a017

Reference yield:

: 2550-26-7
4-Phenyl-2-butanone

: 81602-13-3
*)>-2-hydroxy-5-<1-hydroxy-2-<(1-methyl-3-phenylpropyl)amino>ethyl>benzamide hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: p-TsOH*H₂O / benzene / 14 h / Heating

2: NaBH₄ / methanol / 16 h / Ambient temperature

4: K₂CO₃ / dimethylformamide / 4 h / Ambient temperature

5: NaBH₄ / ethanol / 16 h / Ambient temperature

6: 70 percent / H₂, 1 N aq. HCl / 20percent Pd(OH)2/C / ethanol / 2 h / 2280 Torr / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; hydrogen; potassium carbonate; toluene-4-sulfonic acid; palladium dihydroxide; In methanol; ethanol; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00353a017