(S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate

Base Information

Chemical Name:(S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate
CAS No.:1274699-59-0
Molecular Formula:C₂₁H₃₃NO₇
Molecular Weight:411.496
Hs Code.:

Synonyms:(S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate

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Chemical Property of (S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate

Chemical Property:

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Technology Process of (S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate

There total 1 articles about (S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1274699-57-8
(S)-tert-butyl 4-((R,E)-1-(benzyloxy)-4-hydroxybut-2-en-1-yl)-2,2-dimethyloxazolidine-3-carboxylate

: (S)-tert-butyl 4-((1S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate

: 1274699-59-0
(S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate

Guidance literature:: (S)-tert-butyl 4-((R,E)-1-(benzyloxy)-4-hydroxybut-2-en-1-yl)-2,2-dimethyloxazolidine-3-carboxylate; With osmium(VIII) oxide; citric acid; In water; acetone; at 20 ℃;

With 4-methylmorpholine N-oxide; In water; acetone; at 20 ℃; for 6h; optical yield given as %de;
DOI:10.1039/c0ob00747a

Reference yield: 76.0%

: 1274699-59-0
(S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate

: 98-59-9
p-toluenesulfonyl chloride

: 1274699-61-4
(S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3-dihydroxy-4-(tosyloxy)butyl)-2,2-dimethyloxazolidine-3-carboxylate

Guidance literature:: With 1-methyl-1H-imidazole; In dichloromethane; at 0 ℃; for 4h; Inert atmosphere;
DOI:10.1039/c0ob00747a

Reference yield:

: 1274699-59-0
(S)-tert-butyl 4-((1S,2R,3S)-1-(benzyloxy)-2,3,4-trihydroxybutyl)-2,2-dimethyloxazolidine-3-carboxylate

: 1274699-63-6
C₂₀H₂₇NO₇S

Guidance literature:: Multi-step reaction with 2 steps

1: 1-methyl-1H-imidazole / dichloromethane / 4 h / 0 °C / Inert atmosphere

2: hydrogenchloride / methanol

With 1-methyl-1H-imidazole; hydrogenchloride; In methanol; dichloromethane;
DOI:10.1039/c0ob00747a