2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol

Base Information

Chemical Name:2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol
CAS No.:935527-54-1
Molecular Formula:C₅₉H₈₅NO₈
Molecular Weight:936.326
Hs Code.:

Synonyms:2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol

Suppliers and Price of 2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol

There total 8 articles about 2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 935527-53-0
2-azido-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol

: 935527-54-1
2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethanol; dichloromethane; at 20 ℃;

Reference yield:

: 912814-33-6
(2S,3S,4R)-2-azido-1,3,4-docosanetriol

: 935527-54-1
2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / acetone / 3 h / 20 °C

1.2: 1 h / 20 °C

2.1: tetrabutylammomium bromide / N,N-dimethyl-formamide; toluene / 96 h / Molecular sieve 4A

3.1: hydrogen / Lindlar's catalyst / ethanol; dichloromethane / 20 °C

With sulfuric acid; tetrabutylammomium bromide; hydrogen; Lindlar's catalyst; In ethanol; dichloromethane; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 912814-32-5
(2R,3R,4R)-2-methanesulfonyloxy-1,3,4-docosanetriol

: 935527-54-1
2-amino-1-O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-3,4-O-isopropylidene-D-ribo-1,3,4-docosanetriol

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium azide / N,N-dimethyl-formamide / 20 - 95 °C

2.1: sulfuric acid / acetone / 3 h / 20 °C

2.2: 1 h / 20 °C

3.1: tetrabutylammomium bromide / N,N-dimethyl-formamide; toluene / 96 h / Molecular sieve 4A

4.1: hydrogen / Lindlar's catalyst / ethanol; dichloromethane / 20 °C

With sodium azide; sulfuric acid; tetrabutylammomium bromide; hydrogen; Lindlar's catalyst; In ethanol; dichloromethane; N,N-dimethyl-formamide; acetone; toluene;