5--2-methylmercapto-6-methyl-4-phenylpyrimidine

Base Information

Chemical Name:5--2-methylmercapto-6-methyl-4-phenylpyrimidine
CAS No.:113697-49-7
Molecular Formula:C₁₉H₁₉N₅O₂S
Molecular Weight:381.458
Hs Code.:

5-<N-(4-Amino-3-nitrophenyl)aminomethyl>-2-methylmercapto-6-methyl-4-phenylpyrimidine

Synonyms:5--2-methylmercapto-6-methyl-4-phenylpyrimidine

Suppliers and Price of 5--2-methylmercapto-6-methyl-4-phenylpyrimidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5--2-methylmercapto-6-methyl-4-phenylpyrimidine

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Technology Process of 5--2-methylmercapto-6-methyl-4-phenylpyrimidine

There total 5 articles about 5--2-methylmercapto-6-methyl-4-phenylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5307-14-2,183870-67-9
2-nitro-1,4-phenylenediamine

: 113697-47-5
5-Bromomethyl-2-methylmercapto-6-methyl-4-phenylpyrimidine

: 113697-49-7
5--2-methylmercapto-6-methyl-4-phenylpyrimidine

Guidance literature:: With triethylamine; In benzene; at 25 ℃; for 1h;

Reference yield:

: 123043-88-9,33458-26-3
5-ethoxycarbonyl-4-phenyl-6-methyl-3,4-dihydropyrimidine-2(1H)-thione

: 113697-49-7
5--2-methylmercapto-6-methyl-4-phenylpyrimidine

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / NaOH / methanol / 1 h / 30 °C

2: 70 percent / manganic acetate / benzene / 2.5 h / Heating

3: 25 percent / LAH / diethyl ether / 0.5 h / 5 - 10 °C

4: 65 percent / PBr₃, triethylamine / benzene / 1 h / 25 °C

5: 65 percent / triethylamine / benzene / 1 h / 25 °C

With sodium hydroxide; lithium aluminium tetrahydride; manganese triacetate; phosphorus tribromide; triethylamine; In methanol; diethyl ether; benzene;

Reference yield:

: 74840-45-2
ethyl 6-methyl-2-methylthio-4-phenyl-3,4,5,6-tetrahydropyrimidine-5-carboxylate

: 113697-49-7
5--2-methylmercapto-6-methyl-4-phenylpyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / manganic acetate / benzene / 2.5 h / Heating

2: 25 percent / LAH / diethyl ether / 0.5 h / 5 - 10 °C

3: 65 percent / PBr₃, triethylamine / benzene / 1 h / 25 °C

4: 65 percent / triethylamine / benzene / 1 h / 25 °C

With lithium aluminium tetrahydride; manganese triacetate; phosphorus tribromide; triethylamine; In diethyl ether; benzene;