10β-benzyloxycarbonyl-4β,7-dichloro-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone

Base Information

Chemical Name:10β-benzyloxycarbonyl-4β,7-dichloro-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone
CAS No.:74253-29-5
Molecular Formula:C₂₆H₂₆Cl₂O₄
Molecular Weight:473.396
Hs Code.:

Synonyms:10β-benzyloxycarbonyl-4β,7-dichloro-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone

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Chemical Property of 10β-benzyloxycarbonyl-4β,7-dichloro-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone

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Technology Process of 10β-benzyloxycarbonyl-4β,7-dichloro-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone

There total 3 articles about 10β-benzyloxycarbonyl-4β,7-dichloro-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1178-69-4
benzyl gibberellate

: 74253-29-5
C₂₆H₂₆Cl₂O₄

: 74253-30-8
C₃₀H₃₄Cl₂O₅

Guidance literature:: With N-(2-chloro-1,1,2-trifluoroethyl)diethylamine; lithium chloride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)71418-3

Reference yield:

: 1178-69-4
benzyl gibberellate

: 74253-29-5
10β-benzyloxycarbonyl-4β,7-dichloro-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone

: 74253-30-8
10β-benzyloxycarbonyl-4β-chloro-7α-(4-chloro-n-butoxy)-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone

Guidance literature:: With N-(2-chloro-1,1,2-trifluoroethyl)diethylamine; lithium chloride; In tetrahydrofuran; 1.) 0 deg C, 1h, 2.) room temperature, 1 h;
DOI:10.1039/P19810000098

Reference yield:

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1178-69-4
benzyl gibberellate

: 74253-29-5
10β-benzyloxycarbonyl-4β,7-dichloro-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone

: 74253-30-8
10β-benzyloxycarbonyl-4β-chloro-7α-(4-chloro-n-butoxy)-1β-methyl-8-methylenegibb-2-ene-1α,4aα-carbolactone

Guidance literature:: With N-(2-chloro-1,1,2-trifluoroethyl)diethylamine; lithium chloride; 1.) 0 deg C, 1h, 2.) room temperature, 1 h;
DOI:10.1039/P19810000098