C₂₇H₃₆O₃

Base Information

Chemical Name:C₂₇H₃₆O₃
CAS No.:887502-21-8
Molecular Formula:C₂₇H₃₆O₃
Molecular Weight:408.581
Hs Code.:

C<sub>27</sub>H<sub>36</sub>O<sub>3</sub>

Synonyms:C₂₇H₃₆O₃

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Chemical Property of C₂₇H₃₆O₃

Chemical Property:

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Technology Process of C₂₇H₃₆O₃

There total 9 articles about C₂₇H₃₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 628-71-7
1-Heptyne

: 146072-04-0
(2R,3R)-2,3-Bis-benzyloxy-hexanal

: 887502-21-8
C₂₇H₃₆O₃

Guidance literature:: 1-Heptyne; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;

(2R,3R)-2,3-Bis-benzyloxy-hexanal; In tetrahydrofuran; hexane; at -78 ℃; Further stages.;
DOI:10.1002/chem.200501127

Reference yield:

: C₁₃H₁₈O₃

: 887502-21-8
C₂₇H₃₆O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: NaH / various solvent(s); tetrahydrofuran / 0 °C

1.2: n-Bu₄NI / various solvent(s); tetrahydrofuran / 20 °C

2.1: 7.24 g / 10-camphorsulfonic acid / methanol / 0 °C

3.1: pyridinium 4-toluenesulfonate / CH₂Cl₂ / 6 h / 20 °C

4.1: NaH / various solvent(s); tetrahydrofuran / 0 °C

4.2: n-Bu₄NI / various solvent(s); tetrahydrofuran / 20 °C

5.1: 187 mg / aq. HCl / methanol / 0 °C

6.1: pyridinium chlorochromate; NaOAc / CH₂Cl₂ / 0 °C

7.1: n-BuLi / hexane; tetrahydrofuran / -78 - 20 °C

7.2: hexane; tetrahydrofuran / -78 °C

With hydrogenchloride; n-butyllithium; (1S)-10-camphorsulfonic acid; sodium acetate; pyridinium p-toluenesulfonate; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1002/chem.200501127

Reference yield:

: C₂₀H₂₂O₄

: 887502-21-8
C₂₇H₃₆O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium methoxide / various solvent(s); CH₂Cl₂; methanol / 0.5 h / 0 °C

2.1: NaH / various solvent(s); tetrahydrofuran / 0 °C

2.2: n-Bu₄NI / various solvent(s); tetrahydrofuran / 20 °C

3.1: 7.24 g / 10-camphorsulfonic acid / methanol / 0 °C

4.1: pyridinium 4-toluenesulfonate / CH₂Cl₂ / 6 h / 20 °C

5.1: NaH / various solvent(s); tetrahydrofuran / 0 °C

5.2: n-Bu₄NI / various solvent(s); tetrahydrofuran / 20 °C

6.1: 187 mg / aq. HCl / methanol / 0 °C

7.1: pyridinium chlorochromate; NaOAc / CH₂Cl₂ / 0 °C

8.1: n-BuLi / hexane; tetrahydrofuran / -78 - 20 °C

8.2: hexane; tetrahydrofuran / -78 °C

With hydrogenchloride; n-butyllithium; (1S)-10-camphorsulfonic acid; sodium methylate; sodium acetate; pyridinium p-toluenesulfonate; sodium hydride; pyridinium chlorochromate; In tetrahydrofuran; methanol; hexane; dichloromethane;
DOI:10.1002/chem.200501127