3-Amino-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonylbenzoic acid methyl ester

Base Information

• Chemical Name: 3-Amino-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonylbenzoic acid methyl ester
• CAS No.: 60376-80-9
• Molecular Formula: C₁₇H₁₉N₃O₄S₂
• Molecular Weight: 393.488

Synonyms:3-Amino-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonylbenzoic acid methyl ester

Chemical Property of 3-Amino-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonylbenzoic acid methyl ester

Chemical Property:

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Technology Process of 3-Amino-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonylbenzoic acid methyl ester

There total 2 articles about 3-Amino-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonylbenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3-[(E)-dimethylaminomethyleneamino]sulfonyl-5-nitro-4-phenylsulfanylbenzoate → 3-Amino-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonylbenzoic acid methyl ester (60376-80-9)

Guidance literature:

aluminum nickel; In N,N-dimethyl-formamide;

Reference yield:

→ 3-Amino-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonylbenzoic acid methyl ester (60376-80-9)

Guidance literature:

entspr. Nitro-Verb. (54a), H2 (Ni);

Reference yield: 40.0%

diformylhydrazine (628-36-4) + 3-Amino-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonylbenzoic acid methyl ester (60376-80-9) → 5-Dimethylaminomethylenaminosulfonyl-4-thiophenoxy-3-(1,3,4-triazol-1-yl)benzoesaeuremethylester (86045-23-0)

Guidance literature:

With trichlorophosphate; Heating;

DOI:10.1002/ardp.19833160514

Downstream raw materials:

5-Dimethylaminomethylenaminosulfonyl-4-thiophenoxy-3-(1,3,4-triazol-1-yl)benzoesaeuremethylester

5-Sulfamoyl-4-thiophenoxy-3-(1,3,4-triazol-1-yl)benzoesaeure

3-N-succinimido-4-phenylmercapto-5-N,N-dimethylaminomethyleneaminosulphonyl-benzoic acid methyl ester

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