Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate]

Base Information

Chemical Name:Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate]
CAS No.:1163176-06-4
Molecular Formula:C₁₅H₁₁N₂S*Na
Molecular Weight:274.322
Hs Code.:

Synonyms:Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate]

Suppliers and Price of Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate]

Chemical Property:

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Technology Process of Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate]

There total 4 articles about Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1163176-05-3
2-Chloro-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-3-carbonitrile

: 1163176-06-4
Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate]

Guidance literature:: With sodium sulfide; In N,N-dimethyl-formamide; at 30 ℃; for 5h;

Reference yield:

: 120-92-3
cyclopentanone

: 1163176-06-4
Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate]

Guidance literature:: Multi-step reaction with 3 steps

1: ammonium acetate / toluene / 2 h / Reflux

2: copper dichloride; isopentyl nitrite / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

3: sodium sulfide / N,N-dimethyl-formamide / 5 h / 30 °C

With sodium sulfide; ammonium acetate; copper dichloride; isopentyl nitrite; In tetrahydrofuran; N,N-dimethyl-formamide; toluene;

Reference yield:

: 74873-40-8
2-amino-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-3-carbonitrile

: 1163176-06-4
Sodium [3-cyano-4-phenyl-6,7-dihydro-5H-cyclopenta[b]pyridine-2-thiolate]

Guidance literature:: Multi-step reaction with 2 steps

1: copper dichloride; isopentyl nitrite / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

2: sodium sulfide / N,N-dimethyl-formamide / 5 h / 30 °C

With sodium sulfide; copper dichloride; isopentyl nitrite; In tetrahydrofuran; N,N-dimethyl-formamide;