2-succinimidyloxycarbonyloxy-1,1-dimethylethyl 2-methyl-1-phenylpropyl nitroxide

Base Information

Chemical Name:2-succinimidyloxycarbonyloxy-1,1-dimethylethyl 2-methyl-1-phenylpropyl nitroxide
CAS No.:913816-71-4
Molecular Formula:C₁₉H₂₅N₂O₆
Molecular Weight:377.417
Hs Code.:

Synonyms:2-succinimidyloxycarbonyloxy-1,1-dimethylethyl 2-methyl-1-phenylpropyl nitroxide

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Chemical Property of 2-succinimidyloxycarbonyloxy-1,1-dimethylethyl 2-methyl-1-phenylpropyl nitroxide

Chemical Property:

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Technology Process of 2-succinimidyloxycarbonyloxy-1,1-dimethylethyl 2-methyl-1-phenylpropyl nitroxide

There total 6 articles about 2-succinimidyloxycarbonyloxy-1,1-dimethylethyl 2-methyl-1-phenylpropyl nitroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74124-79-1
di(succinimido) carbonate

: 293328-27-5
N-(1,1-dimethyl-2-hydroxypropyl)-N-(2-methyl-1-phenylpropyl)-N-oxyl

: 913816-71-4
2-succinimidyloxycarbonyloxy-1,1-dimethylethyl 2-methyl-1-phenylpropyl nitroxide

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 16h;
DOI:10.1021/jo061194p

Reference yield:

: 293328-26-4
C₁₇H₂₉NO₂Si

: 913816-71-4
2-succinimidyloxycarbonyloxy-1,1-dimethylethyl 2-methyl-1-phenylpropyl nitroxide

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / tetrahydrofuran

2: 72 percent / O₂; Cu(OAc)2; NH₄OH / methanol

3: 66 percent / Bu₄NF / tetrahydrofuran / 3.5 h

4: Et₃N / acetonitrile / 16 h / 20 °C

With ammonium hydroxide; copper diacetate; tetrabutyl ammonium fluoride; oxygen; triethylamine; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/jo061194p

Reference yield:

: 393110-72-0
N-[2-(tert-butyl-dimethyl-silanyloxy)-1,1-dimethyl-ethyl]-N-(2-methyl-1-phenyl-propyl)-hydroxylamine

: 913816-71-4
2-succinimidyloxycarbonyloxy-1,1-dimethylethyl 2-methyl-1-phenylpropyl nitroxide

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / O₂; Cu(OAc)2; NH₄OH / methanol

2: 66 percent / Bu₄NF / tetrahydrofuran / 3.5 h

3: Et₃N / acetonitrile / 16 h / 20 °C

With ammonium hydroxide; copper diacetate; tetrabutyl ammonium fluoride; oxygen; triethylamine; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/jo061194p