Technology Process of C27H22N2O4
There total 9 articles about C27H22N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: Zn / acetic acid / 100 - 110 °C
2.1: 60 percent / LiN(Si(CH3)3)2
3.1: 100 percent / BF3*Et2O / CH2Cl2
4.1: 99 percent / H2 / Pd/C / tetrahydrofuran
5.1: dimethylformamide / 2 h / 170 °C
6.1: benzoyl chloride / 20 °C
6.2: K2CO3 / diethyl ether / 0.17 h / Heating
With
boron trifluoride diethyl etherate; hydrogen; benzoyl chloride; lithium hexamethyldisilazane; zinc;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570420405
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 60 percent / LiN(Si(CH3)3)2
2.1: 100 percent / BF3*Et2O / CH2Cl2
3.1: 99 percent / H2 / Pd/C / tetrahydrofuran
4.1: dimethylformamide / 2 h / 170 °C
5.1: benzoyl chloride / 20 °C
5.2: K2CO3 / diethyl ether / 0.17 h / Heating
With
boron trifluoride diethyl etherate; hydrogen; benzoyl chloride; lithium hexamethyldisilazane;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570420405
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 100 percent / BF3*Et2O / CH2Cl2
2.1: 99 percent / H2 / Pd/C / tetrahydrofuran
3.1: dimethylformamide / 2 h / 170 °C
4.1: benzoyl chloride / 20 °C
4.2: K2CO3 / diethyl ether / 0.17 h / Heating
With
boron trifluoride diethyl etherate; hydrogen; benzoyl chloride;
palladium on activated charcoal;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570420405