5-methyl-2-(methylsulfonyl)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide

Base Information

Chemical Name:5-methyl-2-(methylsulfonyl)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide
CAS No.:1415694-48-2
Molecular Formula:C₁₅H₁₃N₃O₄S₂
Molecular Weight:363.418
Hs Code.:

Synonyms:5-methyl-2-(methylsulfonyl)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide

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Chemical Property of 5-methyl-2-(methylsulfonyl)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide

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Technology Process of 5-methyl-2-(methylsulfonyl)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide

There total 3 articles about 5-methyl-2-(methylsulfonyl)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1415694-45-9
5-methyl-2-(methylthio)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide

: 1415694-48-2
5-methyl-2-(methylsulfonyl)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide

Guidance literature:: With potassium permanganate; acetic acid; In water; at 20 ℃;
DOI:10.1007/s00044-012-0324-3

Reference yield:

: 43028-63-3
ethyl 2-amino-5-carbamoyl-4-methylthiophene-3-carboxylate

: 1415694-48-2
5-methyl-2-(methylsulfonyl)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 15 h / Reflux

2: sodium hydroxide / water / 5 h / 20 °C

3: potassium permanganate; acetic acid / water / 20 °C

With potassium permanganate; potassium carbonate; acetic acid; sodium hydroxide; In water; acetonitrile;
DOI:10.1007/s00044-012-0324-3

Reference yield:

: 1415694-39-1
2-mercapto-5-methyl-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide

: 1415694-48-2
5-methyl-2-(methylsulfonyl)-4-oxo-3-phenyl-3,4-dihydrothieno[2,3-d]pyrimidine-6-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water / 5 h / 20 °C

2: potassium permanganate; acetic acid / water / 20 °C

With potassium permanganate; acetic acid; sodium hydroxide; In water;
DOI:10.1007/s00044-012-0324-3