Technology Process of C17H19NO6
There total 9 articles about C17H19NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium osmate(VI) dihydrate; sodium periodate;
In
diethyl ether;
at 20 ℃;
for 2.5h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / acetonitrile / 5 h / 13 - 80 °C / Large scale
2: bromobenzene; selenium(IV) oxide / 13 h / 140 °C / Dean-Stark
3: sodium chlorite; aminosulfonic acid / water; acetone / 0.67 h / 20 °C / Cooling with ice
4: ethanol / 7.5 h / 50 - 75 °C
5: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 15 h / 20 °C
6: sodium periodate; potassium osmate(VI) dihydrate / diethyl ether / 2.5 h / 20 °C
With
selenium(IV) oxide; potassium osmate(VI) dihydrate; sodium chlorite; sodium periodate; bromobenzene; aminosulfonic acid; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
diethyl ether; ethanol; water; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bromobenzene; selenium(IV) oxide / 13 h / 140 °C / Dean-Stark
2: sodium chlorite; aminosulfonic acid / water; acetone / 0.67 h / 20 °C / Cooling with ice
3: ethanol / 7.5 h / 50 - 75 °C
4: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 15 h / 20 °C
5: sodium periodate; potassium osmate(VI) dihydrate / diethyl ether / 2.5 h / 20 °C
With
selenium(IV) oxide; potassium osmate(VI) dihydrate; sodium chlorite; sodium periodate; bromobenzene; aminosulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
diethyl ether; ethanol; water; acetone; acetonitrile;