allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Base Information

Chemical Name:allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside
CAS No.:724764-07-2
Molecular Formula:C₅₀H₅₀O₁₂
Molecular Weight:842.94
Hs Code.:

Synonyms:allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Chemical Property of allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

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Technology Process of allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

There total 1 articles about allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 119471-45-3
allyl 3,4-di-O-benzyl-α-L-rhamnosylpyranose

: 206257-92-3
2,3,4-tri-O-benzoyl-α/β-L- rhamnopyranoside trichloroacetimidate

: 724764-07-2
allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In diethyl ether; at -70 - 20 ℃; for 8h;
DOI:10.1039/b400986j

Reference yield: 84.0%

: 724764-07-2
allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-L-rhamnopyranose

Guidance literature:: allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside; With hydrogen; (1,5-cyclooctadiene)[bis(methyldiphenylphosphine)]iridium(I) hexafluorophosphate; In tetrahydrofuran; at 20 ℃;

With mercury dibromide; mercury(II) oxide; In water; acetone; at 20 ℃; for 1h;
DOI:10.1039/b400986j

Reference yield:

: 724764-07-2
allyl 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-α-L-rhamnopyranoside

: 724764-09-4
2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzyl-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / [Ir(COD){PCH₃(C₆H₅)2}](+)*PF₆(-) / tetrahydrofuran / 20 °C

1.2: 84 percent / HgO; HgBr₂ / acetone; H₂O / 1 h / 20 °C

2.1: 96 percent / DBU / CH₂Cl₂ / 2 h / 20 °C

With hydrogen; 1,8-diazabicyclo[5.4.0]undec-7-ene; (1,5-cyclooctadiene)[bis(methyldiphenylphosphine)]iridium(I) hexafluorophosphate; In tetrahydrofuran; dichloromethane;
DOI:10.1039/b400986j