(E)-(5S,6S,7R)-8-Hydroxy-6-(4-methoxy-benzyloxy)-4,5,7-trimethyl-oct-3-enoic acid dimethylamide

Base Information

Chemical Name:(E)-(5S,6S,7R)-8-Hydroxy-6-(4-methoxy-benzyloxy)-4,5,7-trimethyl-oct-3-enoic acid dimethylamide
CAS No.:181644-41-7
Molecular Formula:C₂₁H₃₃NO₄
Molecular Weight:363.497
Hs Code.:

Synonyms:(E)-(5S,6S,7R)-8-Hydroxy-6-(4-methoxy-benzyloxy)-4,5,7-trimethyl-oct-3-enoic acid dimethylamide

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Chemical Property of (E)-(5S,6S,7R)-8-Hydroxy-6-(4-methoxy-benzyloxy)-4,5,7-trimethyl-oct-3-enoic acid dimethylamide

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Technology Process of (E)-(5S,6S,7R)-8-Hydroxy-6-(4-methoxy-benzyloxy)-4,5,7-trimethyl-oct-3-enoic acid dimethylamide

There total 3 articles about (E)-(5S,6S,7R)-8-Hydroxy-6-(4-methoxy-benzyloxy)-4,5,7-trimethyl-oct-3-enoic acid dimethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 181643-93-6
(E)-(S)-5-[(2R,4S,5R)-2-(4-Methoxy-phenyl)-5-methyl-[1,3]dioxan-4-yl]-4-methyl-hex-3-enoic acid dimethylamide

: 181644-41-7
(E)-(5S,6S,7R)-8-Hydroxy-6-(4-methoxy-benzyloxy)-4,5,7-trimethyl-oct-3-enoic acid dimethylamide

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -50 ℃; for 15h;
DOI:10.1021/jo960531z

Reference yield:

: (E)-(S)-3-(Dimethyl-phenyl-silanyl)-4-methyl-hex-4-enoic acid dimethylamide

: 181644-41-7
(E)-(5S,6S,7R)-8-Hydroxy-6-(4-methoxy-benzyloxy)-4,5,7-trimethyl-oct-3-enoic acid dimethylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1) TiCl₄, 2) BCl₃ / 1), 2) PhMe

2: 88 percent / p-TsOH / benzene / Ambient temperature

3: 100 percent / DIBAL-H / CH₂Cl₂ / 15 h / -50 °C

With boron trichloride; titanium tetrachloride; diisobutylaluminium hydride; toluene-4-sulfonic acid; In dichloromethane; benzene;
DOI:10.1021/jo960531z

Reference yield:

: 181643-92-5
(E)-(5S,6S,7R)-6,8-Dihydroxy-4,5,7-trimethyl-oct-3-enoic acid dimethylamide

: 181644-41-7
(E)-(5S,6S,7R)-8-Hydroxy-6-(4-methoxy-benzyloxy)-4,5,7-trimethyl-oct-3-enoic acid dimethylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / p-TsOH / benzene / Ambient temperature

2: 100 percent / DIBAL-H / CH₂Cl₂ / 15 h / -50 °C

With diisobutylaluminium hydride; toluene-4-sulfonic acid; In dichloromethane; benzene;
DOI:10.1021/jo960531z