Technology Process of dodecyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside
There total 6 articles about dodecyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
aluminium trichloride; molecular sieve; tetrafluoroboric acid-diethyl ether complex;
In
tetrahydrofuran;
at 20 ℃;
for 21h;
DOI:10.1016/S0008-6215(02)00294-X
- Guidance literature:
-
Multi-step reaction with 4 steps
1: NaOMe / methanol / 20 °C
2: p-TsOH*H2O / dimethylformamide / 4.5 h / 50 °C
3: 10.1 g / NaH / dimethylformamide / 0 - 20 °C
4: 95 percent / BH3*Et2O; AlCl3; molecular sieves / tetrahydrofuran / 21 h / 20 °C
With
aluminium trichloride; molecular sieve; tetrafluoroboric acid-diethyl ether complex; sodium methylate; sodium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(02)00294-X
- Guidance literature:
-
Multi-step reaction with 5 steps
1: silver perchlorate; silver carbonate; molecular sieves / CH2Cl2
2: NaOMe / methanol / 20 °C
3: p-TsOH*H2O / dimethylformamide / 4.5 h / 50 °C
4: 10.1 g / NaH / dimethylformamide / 0 - 20 °C
5: 95 percent / BH3*Et2O; AlCl3; molecular sieves / tetrahydrofuran / 21 h / 20 °C
With
aluminium trichloride; molecular sieve; tetrafluoroboric acid-diethyl ether complex; sodium methylate; silver perchlorate; sodium hydride; toluene-4-sulfonic acid; silver carbonate;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(02)00294-X
