tetra-O-acetyl-4-O-benzyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol

Base Information

• Chemical Name: tetra-O-acetyl-4-O-benzyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol
• CAS No.: 952723-26-1
• Molecular Formula: C₃₅H₄₄O₁₉
• Molecular Weight: 768.723

Synonyms:tetra-O-acetyl-4-O-benzyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol

Chemical Property of tetra-O-acetyl-4-O-benzyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of tetra-O-acetyl-4-O-benzyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol

There total 1 articles about tetra-O-acetyl-4-O-benzyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-benzyloxy-6-(3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-cyclohexane-1,2,4,5-tetraol + acetic anhydride (108-24-7) → tetra-O-acetyl-4-O-benzyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol (952723-26-1)

Guidance literature:

With pyridine; dmap; at 50 ℃; for 3h;

DOI:10.1071/CH06393

Reference yield: 87.0%

tetra-O-acetyl-4-O-benzyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol (952723-26-1) → tetra-O-acetyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; for 24h;

DOI:10.1071/CH06393

Reference yield:

tetra-O-acetyl-4-O-benzyl-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol (952723-26-1) → tetra-O-acetyl-4-O-(4-methylphenylsulfonyl)-1-O-(tetra-O-acetyl-β-D-galactopyranosyl)-scyllo-inositol

Guidance literature:

Multi-step reaction with 2 steps

1: 87 percent / H₂ / palladium on activated charcoal / tetrahydrofuran; methanol / 24 h

2: 87 percent / pyridine / H₂O / 2 h / 50 °C

With pyridine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; water;

DOI:10.1071/CH06393

upstream raw materials:

acetic anhydride

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