C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi

Base Information

Chemical Name:C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi
CAS No.:1254691-05-8
Molecular Formula:C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi
Molecular Weight:732.16
Hs Code.:

C<sub>2</sub>H<sub>4</sub>O<sub>2</sub>*C<sub>27</sub>H<sub>33</sub>Cl<sub>3</sub>N<sub>6</sub>O<sub>4</sub>SSi

Synonyms:C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi

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Chemical Property of C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi

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Technology Process of C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi

There total 7 articles about C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1061574-19-3
C₃₀H₃₇Cl₃N₄O₅S₂Si

: 1254691-05-8
C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi

Guidance literature:: With ammonium acetate; ammonia; In methanol; at 70 ℃; for 24h; vessel sealed with Teflon screw-cap;

Reference yield: 85.0%

: 1061574-19-3
C₃₀H₃₇Cl₃N₄O₅S₂Si

: 631-61-8,92206-38-7
ammonium acetate

: 1254691-05-8
C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi

Guidance literature:: With ammonia; In methanol; at 70 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.6b02343

Reference yield:

: 1061574-11-5
C₉H₁₂N₂O₄

: 1254691-05-8
C₂H₄O₂*C₂₇H₃₃Cl₃N₆O₄SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 14 h / 0 °C / Inert atmosphere

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 2 h / -90 °C / Inert atmosphere

3.1: dichloromethane / 0.33 h / 0 - 20 °C / Inert atmosphere

3.2: 1.67 h / -78 - 20 °C / Inert atmosphere

4.1: 1,3-dimethylbarbituric acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 8 h / Inert atmosphere

4.2: 0.33 h / Inert atmosphere

5.1: 2,4,6-tri-tert-butylpyrimidine / dichloromethane / 29 h / 37 °C / Inert atmosphere; Sealed tube

6.1: ammonia / methanol / 24 h / 70 °C / Inert atmosphere; Sealed tube

With 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; ammonia; diisobutylaluminium hydride; 2,4,6-tri-tert-butylpyrimidine; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; 3.1: |Pictet-Spengler Synthesis / 3.2: |Pictet-Spengler Synthesis;
DOI:10.1021/jacs.6b02343