6-acetylamino-1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2-one

Base Information

Chemical Name:6-acetylamino-1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2-one
CAS No.:133150-07-9
Molecular Formula:C₂₂H₂₄N₂O₄S
Molecular Weight:412.51
Hs Code.:

Synonyms:6-acetylamino-1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2-one

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Chemical Property of 6-acetylamino-1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2-one

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Technology Process of 6-acetylamino-1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2-one

There total 3 articles about 6-acetylamino-1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 108-24-7
acetic anhydride

: 133150-06-8
1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2,6-dione-6-oxime

: 133150-07-9
6-acetylamino-1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetic acid; for 2h;

Reference yield:

: 133150-03-5
1,5-dimethyl-5-<4-(phenylthio)phenyl>-dihydro<1H,7H>-5H-pyrano<3,2-d>oxazole-2,6-dione

: 133150-07-9
6-acetylamino-1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / NH₂OH*HCl, NaOAc / methanol / 12 h / 40 °C

2: 84 percent / H₂ / 10percent Pd/C / acetic acid / 2 h

With hydroxylamine hydrochloride; hydrogen; sodium acetate; palladium on activated charcoal; In methanol; acetic acid;

Reference yield:

: 133150-04-6,145371-47-7
2--2-methyl-6-<<(methylamino)carbonyl>oxy>-3-oxo-3,6-dihydro-2H-pyran

: 133150-07-9
6-acetylamino-1,5-dimethyl-5<4-(phenylthio)phenyl>perhydropyrano<3,2-d>oxazole-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / aq. Na₂CO₃ / 0.25 h / 5 °C

2: 88 percent / NH₂OH*HCl, NaOAc / methanol / 12 h / 40 °C

3: 84 percent / H₂ / 10percent Pd/C / acetic acid / 2 h

With hydroxylamine hydrochloride; hydrogen; sodium acetate; sodium carbonate; palladium on activated charcoal; In methanol; acetic acid;