3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Base Information

Chemical Name:3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate
CAS No.:1407188-03-7
Molecular Formula:C₄₂H₄₀BrF₂₆NO₆S₂
Molecular Weight:1292.78
Hs Code.:

3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Synonyms:3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

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Chemical Property of 3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

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Technology Process of 3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

There total 9 articles about 3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1407187-98-7
3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

: 1,2-bis(bromomethyl)-4,5-dipropylbenzene

: 1407188-03-7
3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol302748h

Reference yield:

: 1176082-82-8
4,5-dipropylphthalic acid dimethyl ester

: 1407188-03-7
3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

2: phosphorus tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; phosphorus tribromide; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol302748h

Reference yield:

: 1008093-86-4
1,2-bis(hydroxymethyl)-4,5-dipropylbenzene

: 1407188-03-7
3-(2-(bromomethyl)-4,5-dipropylbenzyl)-3-((3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)sulfonyl)-1-hexyl-2-oxoindolin-6-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With phosphorus tribromide; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol302748h