2-<2-(N,N-dibenzoyl)carbamoylethyl>-1-(methoxycarbonylmethyl)azetidinone

Base Information

Chemical Name:2-<2-(N,N-dibenzoyl)carbamoylethyl>-1-(methoxycarbonylmethyl)azetidinone
CAS No.:136810-40-7
Molecular Formula:C₂₃H₂₂N₂O₆
Molecular Weight:422.437
Hs Code.:

Synonyms:2-<2-(N,N-dibenzoyl)carbamoylethyl>-1-(methoxycarbonylmethyl)azetidinone

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Chemical Property of 2-<2-(N,N-dibenzoyl)carbamoylethyl>-1-(methoxycarbonylmethyl)azetidinone

Chemical Property:

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Technology Process of 2-<2-(N,N-dibenzoyl)carbamoylethyl>-1-(methoxycarbonylmethyl)azetidinone

There total 8 articles about 2-<2-(N,N-dibenzoyl)carbamoylethyl>-1-(methoxycarbonylmethyl)azetidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 129374-54-5
2-<2-(4,5-diphenyl-2-oxazolyl)ethyl>-1-(methoxycarbonylmethyl)azetidinone

: 136810-40-7
2-<2-(N,N-dibenzoyl)carbamoylethyl>-1-(methoxycarbonylmethyl)azetidinone

Guidance literature:: With Sensitox; oxygen; In dichloromethane; for 3h; Irradiation;

Reference yield:

: 21256-18-8
3-(4,5-Diphenyl-oxazol-2-yl)-propionic acid

: 136810-40-7
2-<2-(N,N-dibenzoyl)carbamoylethyl>-1-(methoxycarbonylmethyl)azetidinone

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) carbonyldiimidazole / 1.) THF, 25 deg C, 6 h, 2.) 25 deg C

2: 80 percent / ammonium acetate, acetic acid / benzene / 3 h / Heating

3: 87 percent / concd. HCl, NaBH₃CN, Bromokresol Green / tetrahydrofuran; ethanol / 0 °C

4: 87.8 percent / NaOH / methanol / 4 h / Heating

5: 74 percent / H₂O; ethane-1,2-diol; glycerol / 2.5 h / 25 °C

6: 85 percent / DMAP / acetonitrile / 4.5 h / 25 °C

7: 2.) Me₃SiOSO₂CF₃ / 1.) CH₃OH, 0 deg C, 3 min, 2.) benzene, 25 deg C, 5 min

8: O₂, Sensitox / CH₂Cl₂ / 3 h / Irradiation

With ammonium acetate; hydrogenchloride; dmap; sodium hydroxide; trimethylsilyl trifluoromethanesulfonate; Sensitox; oxygen; bromocresol green; sodium cyanoborohydride; acetic acid; 1,1'-carbonyldiimidazole; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; ethylene glycol; glycerol; acetonitrile; benzene;

Reference yield:

: 129374-51-2
5-(4,5-diphenyl-2-oxazolyl)-3-aminopentanoic acid

: 136810-40-7
2-<2-(N,N-dibenzoyl)carbamoylethyl>-1-(methoxycarbonylmethyl)azetidinone

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / H₂O; ethane-1,2-diol; glycerol / 2.5 h / 25 °C

2: 85 percent / DMAP / acetonitrile / 4.5 h / 25 °C

3: 2.) Me₃SiOSO₂CF₃ / 1.) CH₃OH, 0 deg C, 3 min, 2.) benzene, 25 deg C, 5 min

4: O₂, Sensitox / CH₂Cl₂ / 3 h / Irradiation

With dmap; trimethylsilyl trifluoromethanesulfonate; Sensitox; oxygen; In dichloromethane; water; ethylene glycol; glycerol; acetonitrile;