methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-β-D-glucopyranosyloxy)benzoate

Base Information

Chemical Name:methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-β-D-glucopyranosyloxy)benzoate
CAS No.:1293384-37-8
Molecular Formula:C₃₆H₃₈O₉
Molecular Weight:614.692
Hs Code.:

Synonyms:methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-β-D-glucopyranosyloxy)benzoate

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Chemical Property of methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-β-D-glucopyranosyloxy)benzoate

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Technology Process of methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-β-D-glucopyranosyloxy)benzoate

There total 6 articles about methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-β-D-glucopyranosyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1293384-35-6
methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-6'-O-trityl-β-D-glucopyranosyloxy)benzoate

: 1293384-37-8
methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-β-D-glucopyranosyloxy)benzoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; water; at 0 ℃; for 0.5h;
DOI:10.1021/jo200440r

Reference yield:

: 942428-83-3
2,3,4,6-tetra-O-acetyl-D-glucopyranosyl 1-(N-phenyl)-2,2,2-trifluoroacetimidate

: 1293384-37-8
methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-β-D-glucopyranosyloxy)benzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C

2.1: potassium carbonate / tetrahydrofuran; methanol / 20 °C

3.1: dmap / pyridine / 5 h / 55 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C

4.2: 3 h / 20 °C

5.1: trifluoroacetic acid / dichloromethane; water / 0.5 h / 0 °C

With dmap; boron trifluoride diethyl etherate; sodium hydride; potassium carbonate; trifluoroacetic acid; In tetrahydrofuran; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo200440r

Reference yield:

: 1293384-36-7
methyl 3-methoxy-4-(6'-O-trityl-β-D-glucopyranosyloxy)benzoate

: 1293384-37-8
methyl 3-methoxy-4-(2',3',4'-tri-O-benzyl-β-D-glucopyranosyloxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 0 °C

1.2: 3 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane; water / 0.5 h / 0 °C

With sodium hydride; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jo200440r