2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine

Base Information

Chemical Name:2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine
CAS No.:76051-36-0
Molecular Formula:C₂₈H₃₆N₂O₁₄
Molecular Weight:624.599
Hs Code.:

Synonyms:2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine

Suppliers and Price of 2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine

There total 3 articles about 2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4668-43-3
(S)-3-(benzyloxycarbonylamino)-4-ethoxy-4-oxobutanoic acid

: 70128-27-7
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosylamine

: 76051-36-0
2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine

Guidance literature:: With diethyl cyanophosphonate; triethylamine; In tetrahydrofuran; at 0 ℃; for 12h;
DOI:10.1139/v80-415

Reference yield:

: 4451-36-9
2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl chloride

: 76051-36-0
2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / sodium azide / hexamethylphosphoric acid triamide / 3.5 h

2: 21 percent / hydrogen / Adams' catalyst / methanol / 13 h / Ambient temperature

3: 90 percent / diethyl phosphorocyanidate, triethylamine / tetrahydrofuran / 12 h / 0 °C

With sodium azide; diethyl cyanophosphonate; hydrogen; triethylamine; platinum(IV) oxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide;
DOI:10.1139/v80-415

Reference yield:

: 20379-61-7
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl azide

: 76051-36-0
2,3,4,6-tetra-O-acetyl-N-(α-ethyl benzyloxycarbonyl-L-aspartyl)-α-D-glucopyranosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 21 percent / hydrogen / Adams' catalyst / methanol / 13 h / Ambient temperature

2: 90 percent / diethyl phosphorocyanidate, triethylamine / tetrahydrofuran / 12 h / 0 °C

With diethyl cyanophosphonate; hydrogen; triethylamine; platinum(IV) oxide; In tetrahydrofuran; methanol;
DOI:10.1139/v80-415