N-Benzyl-N-[(S)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-furan-2-yl-methyl]-hydroxylamine

Base Information

Chemical Name:N-Benzyl-N-[(S)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-furan-2-yl-methyl]-hydroxylamine
CAS No.:152390-88-0
Molecular Formula:C₁₇H₂₁NO₄
Molecular Weight:303.358
Hs Code.:

Synonyms:N-Benzyl-N-[(S)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-furan-2-yl-methyl]-hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-Benzyl-N-[(S)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-furan-2-yl-methyl]-hydroxylamine

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Technology Process of N-Benzyl-N-[(S)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-furan-2-yl-methyl]-hydroxylamine

There total 2 articles about N-Benzyl-N-[(S)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-furan-2-yl-methyl]-hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 2786-02-9
2-lithiofuran

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-2,3-O-isopropylidene-D-glyceraldehyde nitrone

: 152390-88-0
N-Benzyl-N-[(S)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-furan-2-yl-methyl]-hydroxylamine

: 152390-89-1
N-Benzyl-N-[(R)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-furan-2-yl-methyl]-hydroxylamine

Guidance literature:: In tetrahydrofuran; at -80 ℃; for 0.5h; Yields of byproduct given;
DOI:10.1055/s-1994-25712

Reference yield:

: 110-00-9
furan

: 91190-38-4,111058-38-9,1165677-00-8
N-benzyl-1,2-O-isopropylidene-D-glyceraldehyde nitrone

: 152390-88-0
N-Benzyl-N-[(S)-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-furan-2-yl-methyl]-hydroxylamine

Guidance literature:: furan; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 2h; Inert atmosphere;

N-benzyl-1,2-O-isopropylidene-D-glyceraldehyde nitrone; In tetrahydrofuran; pentane; at -78 ℃; for 2.25h; optical yield given as %de; Inert atmosphere;
DOI:10.3762/bjoc.6.75