methyl O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Base Information

• Chemical Name: methyl O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
• CAS No.: 104495-23-0
• Molecular Formula: C₅₅H₆₀O₁₀
• Molecular Weight: 881.075

Synonyms:methyl O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Chemical Property of methyl O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

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Technology Process of methyl O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

There total 5 articles about methyl O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

2,3,4-tri-O-benzyl-L-rhamnopyranose (210426-02-1) + methyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside (19488-49-4) → methyl O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside (104495-23-0) + methyl O-(2,3,4-tri-O-benzyl-β-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside

Guidance literature:

With trimethylsilyl bromide; tetrabutylammomium bromide; cobalt(II) bromide; 4 A molecular sieve; In 1,2-dichloro-ethane; at 25 ℃;

DOI:10.1246/bcsj.74.1679

Reference yield: 69.24%

methyl 3,4,6-tri-O-benzyl-β-D-glucopyranoside (720684-67-3) + 2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl fluoride → methyl O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside (104495-23-0)

Guidance literature:

With 4 A molecular sieve; silver perchlorate; tin(ll) chloride; In methanol; diethyl ether; at -15 ℃; for 24h;

Reference yield: 36.0%

2,3,4-tri-O-benzyl-L-rhamnopyranose (210426-02-1) + methyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside (19488-49-4) → methyl O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside (104495-23-0) + O-(2,3,4-tri-O-benzyl-α-L-rhamnopyranosyl)-(1->1)-2,3,4-tri-O-benzyl-α-L-rhamnopyranoside (120269-13-8)

Guidance literature:

With silver trifluoromethanesulfonate; triethylamine; In dichloromethane;

DOI:10.1246/bcsj.61.3943

upstream raw materials:

2,3,4-tri-O-benzyl-L-rhamnopyranose

methyl 2,3,6-tri-O-benzyl-β-D-glucopyranoside

methyl 3,4,6-tri-O-benzyl-β-D-glucopyranoside

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