[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine

Base Information

Chemical Name:[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine
CAS No.:176848-91-2
Molecular Formula:C₂₀H₃₅NOSi₂
Molecular Weight:361.675
Hs Code.:

Synonyms:[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine

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Chemical Property of [1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine

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Technology Process of [1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine

There total 2 articles about [1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 135-02-4
ortho-anisaldehyde

: 176848-87-6
5-Trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enylamine

: 176848-91-2
[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine

Guidance literature:: With 4 A molecular sieve; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/ja954136m

Reference yield:

: 176848-86-5
2-(5-Trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-isoindole-1,3-dione

: 176848-91-2
[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: N₂H₄*H₂O / ethanol / Heating

2: 100 percent / 4A molecular sieves / tetrahydrofuran / Ambient temperature

With 4 A molecular sieve; hydrazine hydrate; In tetrahydrofuran; ethanol;
DOI:10.1021/ja954136m

Reference yield:

: 176848-91-2
[1-(2-Methoxy-phenyl)-meth-(E)-ylidene]-(5-trimethylsilanyl-4-trimethylsilanylmethyl-pent-3-enyl)-amine

: (2R,3S)-2-(2-Methoxy-phenyl)-1-(toluene-4-sulfonyl)-3-(1-trimethylsilanylmethyl-vinyl)-pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) TiCl₄, 2.) aq. KHCO₃ / 1.) CH₂Cl₂, toluene, from -78 deg C, to RT, 5 h, 2.) CH₂Cl₂, toluene, RT, 30 min

2: pyridine / CH₂Cl₂ / 0 - 20 °C

With pyridine; titanium tetrachloride; potassium hydrogencarbonate; In dichloromethane;
DOI:10.1021/ja954136m