2-deuterio-3,5-bis(phenylsulfonyl)-1-benzyl-2-phenyl-1,2,5,6-tetrahydropyridine

Base Information

Chemical Name:2-deuterio-3,5-bis(phenylsulfonyl)-1-benzyl-2-phenyl-1,2,5,6-tetrahydropyridine
CAS No.:133167-15-4
Molecular Formula:C₃₀H₂₇NO₄S₂
Molecular Weight:530.673
Hs Code.:

Synonyms:2-deuterio-3,5-bis(phenylsulfonyl)-1-benzyl-2-phenyl-1,2,5,6-tetrahydropyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-deuterio-3,5-bis(phenylsulfonyl)-1-benzyl-2-phenyl-1,2,5,6-tetrahydropyridine

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Technology Process of 2-deuterio-3,5-bis(phenylsulfonyl)-1-benzyl-2-phenyl-1,2,5,6-tetrahydropyridine

There total 3 articles about 2-deuterio-3,5-bis(phenylsulfonyl)-1-benzyl-2-phenyl-1,2,5,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 85540-20-1
2,3-bis(phenylsulfonyl)-1,3-butadiene

: 910541-44-5
N-(1-deuteriobenzylidene)benzylamine

: 133167-15-4
2-deuterio-3,5-bis(phenylsulfonyl)-1-benzyl-2-phenyl-1,2,5,6-tetrahydropyridine

Guidance literature:: In dichloromethane; at 25 ℃; for 20h;
DOI:10.1021/jo00008a026

Reference yield:

: 85540-18-7
2,3-bis(phenylsulfinyl)-1,3-butadiene

: 133167-15-4
2-deuterio-3,5-bis(phenylsulfonyl)-1-benzyl-2-phenyl-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 1) 0 deg C, 2h, 2) 25 deg C, 8h

2: 81 percent / CH₂Cl₂ / 20 h / 25 °C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo00008a026

Reference yield:

: 108-98-5
thiophenol

: 133167-15-4
2-deuterio-3,5-bis(phenylsulfonyl)-1-benzyl-2-phenyl-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 1) N-chlorosuccinimide, 2) triethylamine / 1) methylene chloride, a) reflux, 5 min, b) 25 deg C, 30 min, 2) -78 deg C, 1h

2: 79 percent / m-chloroperoxybenzoic acid / CH₂Cl₂ / 1) 0 deg C, 2h, 2) 25 deg C, 8h

3: 81 percent / CH₂Cl₂ / 20 h / 25 °C

With N-chloro-succinimide; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jo00008a026