(+/-)-1,2-O-di-n-heptyl-3-O-[4-(N-hydroxylamidino)methylphenyl]glycerol

Base Information

Chemical Name:(+/-)-1,2-O-di-n-heptyl-3-O-[4-(N-hydroxylamidino)methylphenyl]glycerol
CAS No.:945214-32-4
Molecular Formula:C₂₅H₄₄N₂O₄
Molecular Weight:436.635
Hs Code.:

Synonyms:(+/-)-1,2-O-di-n-heptyl-3-O-[4-(N-hydroxylamidino)methylphenyl]glycerol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-1,2-O-di-n-heptyl-3-O-[4-(N-hydroxylamidino)methylphenyl]glycerol

Chemical Property:

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Technology Process of (+/-)-1,2-O-di-n-heptyl-3-O-[4-(N-hydroxylamidino)methylphenyl]glycerol

There total 10 articles about (+/-)-1,2-O-di-n-heptyl-3-O-[4-(N-hydroxylamidino)methylphenyl]glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 935851-86-8
(+/-)-3-O-(4-cyanomethylphenyl)-1,2-O-di-n-heptylglycerol

: 945214-32-4
(+/-)-1,2-O-di-n-heptyl-3-O-[4-(N-hydroxylamidino)methylphenyl]glycerol

Guidance literature:: With hydroxylamine hydrochloride; potassium carbonate; In ethanol; for 18h; Heating;
DOI:10.1021/jm060082n

Reference yield:

: 935851-82-4
(+/-)-1-O-[4-(tetrahydropyran-2-yloxymethyl)phenyl]glycerol

: 945214-32-4
(+/-)-1,2-O-di-n-heptyl-3-O-[4-(N-hydroxylamidino)methylphenyl]glycerol

Guidance literature:: Multi-step reaction with 5 steps

1.1: NaH / dimethylformamide / 1 h / 20 °C

1.2: 55 percent / dimethylformamide / 12 h / 20 °C

2.1: 100 percent / ethanol / pyridinium p-toluenesulfonate / 12 h / 60 °C

3.1: acetic acid; HBr / 0.5 h / 20 °C

4.1: 1.2 g / dimethylformamide / 12 h / 20 °C

5.1: 55 percent / hydroxylamine hydrochloride; K₂CO₃ / ethanol / 18 h / Heating

With ethanol; hydroxylamine hydrochloride; hydrogen bromide; sodium hydride; potassium carbonate; acetic acid; pyridinium p-toluenesulfonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060082n

Reference yield:

: 935851-85-7
(+/-)-1,2-O-di-n-heptyl-3-O-[4-(tetrahydropyran-2-yloxymethyl)phenyl]glycerol

: 945214-32-4
(+/-)-1,2-O-di-n-heptyl-3-O-[4-(N-hydroxylamidino)methylphenyl]glycerol

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / ethanol / pyridinium p-toluenesulfonate / 12 h / 60 °C

2: acetic acid; HBr / 0.5 h / 20 °C

3: 1.2 g / dimethylformamide / 12 h / 20 °C

4: 55 percent / hydroxylamine hydrochloride; K₂CO₃ / ethanol / 18 h / Heating

With ethanol; hydroxylamine hydrochloride; hydrogen bromide; potassium carbonate; acetic acid; pyridinium p-toluenesulfonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060082n