N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N-benzylimidazolium tetrafluoroborate

Base Information

Chemical Name:N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N-benzylimidazolium tetrafluoroborate
CAS No.:1419605-74-5
Molecular Formula:BF₄*C₂₁H₂₁N₄
Molecular Weight:416.229
Hs Code.:

Synonyms:N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N-benzylimidazolium tetrafluoroborate

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Chemical Property of N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N-benzylimidazolium tetrafluoroborate

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Technology Process of N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N-benzylimidazolium tetrafluoroborate

There total 5 articles about N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N-benzylimidazolium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 13826-83-0
ammonium tetrafluroborate

: 1419605-69-8
N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N'-benzylimidazolium chloride

: 1419605-74-5
N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N-benzylimidazolium tetrafluoroborate

Guidance literature:: In water; at 20 ℃; for 0.5h;
DOI:10.1016/j.jorganchem.2012.12.008

Reference yield:

: 50914-15-3
(2-iodophenyl)hydrazine

: 1419605-74-5
N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N-benzylimidazolium tetrafluoroborate

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride / water / 2 h / 20 °C

2: potassium carbonate; L-proline; copper(l) iodide / dimethyl sulfoxide / 48 h / 90 °C / Inert atmosphere

3: potassium carbonate; L-proline; copper(l) iodide / dimethyl sulfoxide / 48 h / 90 °C / Inert atmosphere

4: acetonitrile / 24 h / Reflux

5: water / 0.5 h / 20 °C

With hydrogenchloride; copper(l) iodide; potassium carbonate; L-proline; In water; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.jorganchem.2012.12.008

Reference yield:

: 1419605-60-9
1-(2-iodophenyl)-1H-pyrazole

: 1419605-74-5
N-[2-(3,5-dimethylpyrazol-1-yl)phenyl]-N-benzylimidazolium tetrafluoroborate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; L-proline; copper(l) iodide / dimethyl sulfoxide / 48 h / 90 °C / Inert atmosphere

2: potassium carbonate; L-proline; copper(l) iodide / dimethyl sulfoxide / 48 h / 90 °C / Inert atmosphere

3: acetonitrile / 24 h / Reflux

4: water / 0.5 h / 20 °C

With copper(l) iodide; potassium carbonate; L-proline; In water; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/j.jorganchem.2012.12.008