N-<5-<3-propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

Base Information

Chemical Name:N-<5-<3-propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid
CAS No.:112139-67-0
Molecular Formula:C₄₈H₆₉N₅O₈
Molecular Weight:844.105
Hs Code.:

N-<5-<3-<heptyl(benzyloxy)carbamoyl>propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

Synonyms:N-<5-<3-propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

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Chemical Property of N-<5-<3-propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

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Technology Process of N-<5-<3-propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

There total 9 articles about N-<5-<3-propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 112139-66-9
N-heptyl-N-(benzyloxy)succinamic acid

: 112139-64-7
N-(5-aminopentyl)-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

: 112139-67-0
N-<5-<3-propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 20h; Ambient temperature;
DOI:10.1021/jo00249a001

Reference yield:

: 112139-59-0
O-benzyl-N-(4-cyanobutyl)-hydroxylamine

: 112139-67-0
N-<5-<3-propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / pyridine / 1.5 h / 100 °C

2: 98 percent / DCC, DMAP / CHCl₃ / 24.5 h / 0 - 20 °C

3: 82 percent / H₂, NH₃ / Raney Ni / methanol; H₂O / 2.5 h / 2585.7 Torr

4: 73 percent / DCC, DMAP / CH₂Cl₂ / 20 h / Ambient temperature

With pyridine; dmap; ammonia; hydrogen; dicyclohexyl-carbodiimide; nickel; In methanol; dichloromethane; chloroform; water;
DOI:10.1021/jo00249a001

Reference yield:

: 5-[(E)-Benzyloxyimino]-pentanenitrile

: 112139-67-0
N-<5-<3-propionamido>pentyl>-3-<<5-<(benzyloxy)acetylamino>pentyl>carbamoyl>-O-benzylpropionohydroxamic acid

Guidance literature:: Multi-step reaction with 5 steps

1: sodium cyanoborohydride, HCl / methanol; H₂O / 3 h / Ambient temperature

2: 98 percent / pyridine / 1.5 h / 100 °C

3: 98 percent / DCC, DMAP / CHCl₃ / 24.5 h / 0 - 20 °C

4: 82 percent / H₂, NH₃ / Raney Ni / methanol; H₂O / 2.5 h / 2585.7 Torr

5: 73 percent / DCC, DMAP / CH₂Cl₂ / 20 h / Ambient temperature

With pyridine; hydrogenchloride; dmap; ammonia; hydrogen; sodium cyanoborohydride; dicyclohexyl-carbodiimide; nickel; In methanol; dichloromethane; chloroform; water;
DOI:10.1021/jo00249a001