(2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one

Base Information

Chemical Name:(2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one
CAS No.:917380-33-7
Molecular Formula:C₃₉H₆₈O₄Si₃
Molecular Weight:685.223
Hs Code.:

Synonyms:(2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one

Suppliers and Price of (2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one

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Technology Process of (2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one

There total 1 articles about (2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: (2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undec-3-yn-5-one

: 917380-33-7
(2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one

Guidance literature:: With hydrogen; potassium carbonate; platinum(IV) oxide; In tetrahydrofuran; methanol; for 6h;
DOI:10.1039/b709932k

Reference yield: 93.0%

: 917380-33-7
(2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one

: 917380-38-2
(2S,7S)-7-(3'-(tert-butyldiphenylsilyloxy)-propyl)-2-methyl-1,6-dioxaspiro[4.4]nonane

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1039/b612757f

Reference yield:

: 917380-33-7
(2S,8S)-2,8-bis(tert-butyldimethylsilyloxy)-11-(tert-butyldiphenylsilyloxy)undecan-5-one

: (2S,5S,7S)-7-(3'-(tert-butyldiphenylsilyloxy)-propyl)-2-methyl-1,6-dioxaspiro[4.4]nonane

: (2S,5R,7S)-7-(3'-(tert-butyldiphenylsilyloxy)-propyl)-2-methyl-1,6-dioxaspiro[4.4]nonane

Guidance literature:: With camphorsulfonic cid; In dichloromethane; at 20 ℃; for 4h; Title compound not separated from byproducts.;
DOI:10.1039/b709932k