C₂₈H₂₂FNO₃

Base Information

Chemical Name:C₂₈H₂₂FNO₃
CAS No.:1373241-90-7
Molecular Formula:C₂₈H₂₂FNO₃
Molecular Weight:439.486
Hs Code.:

C<sub>28</sub>H<sub>22</sub>FNO<sub>3</sub>

Synonyms:C₂₈H₂₂FNO₃

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Chemical Property of C₂₈H₂₂FNO₃

Chemical Property:

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Technology Process of C₂₈H₂₂FNO₃

There total 8 articles about C₂₈H₂₂FNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 1373241-87-2
C₂₈H₂₄FNO₄

: 1373241-90-7
C₂₈H₂₂FNO₃

Guidance literature:: C₂₈H₂₄FNO₄; With diethylamino-sulfur trifluoride; In dichloromethane; at -78 - 20 ℃; for 3h; Inert atmosphere;

With water; In dichloromethane;

Reference yield:

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 1373241-90-7
C₂₈H₂₂FNO₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 3 h / 20 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 1 h / 0 °C

2.2: 15 h / 0 - 20 °C

3.1: trifluoroacetic acid; triethylsilane / dichloromethane / 3 h / 0 - 10 °C

4.1: caesium carbonate / tetrahydrofuran / 0.5 h / 20 °C

4.2: 15 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.5 h / -78 - 0 °C / Inert atmosphere

5.2: -40 °C

6.1: aluminum (III) chloride / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere

6.2: 0 °C

7.1: pyrrolidine / methanol / 0.5 h / 20 °C / Inert atmosphere

7.2: 16 h / Reflux; Inert atmosphere

8.1: sodium tetrahydroborate; methanol / 16 h / 0 - 20 °C / Inert atmosphere

9.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / -78 - 20 °C / Inert atmosphere

With pyrrolidine; methanol; triethylsilane; aluminum (III) chloride; sodium tetrahydroborate; diethylamino-sulfur trifluoride; isopropylmagnesium chloride; boron tribromide; sodium hydride; caesium carbonate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 459-46-1
4-Fluorobenzyl bromide

: 1373241-90-7
C₂₈H₂₂FNO₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 3 h / 20 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 1 h / 0 °C

2.2: 15 h / 0 - 20 °C

3.1: trifluoroacetic acid; triethylsilane / dichloromethane / 3 h / 0 - 10 °C

4.1: caesium carbonate / tetrahydrofuran / 0.5 h / 20 °C

4.2: 15 h / 20 °C

5.1: boron tribromide / dichloromethane / 0.5 h / -78 - 0 °C / Inert atmosphere

5.2: -40 °C

6.1: aluminum (III) chloride / dichloromethane / 48 h / 0 - 20 °C / Inert atmosphere

6.2: 0 °C

7.1: pyrrolidine / methanol / 0.5 h / 20 °C / Inert atmosphere

7.2: 16 h / Reflux; Inert atmosphere

8.1: sodium tetrahydroborate; methanol / 16 h / 0 - 20 °C / Inert atmosphere

9.1: diethylamino-sulfur trifluoride / dichloromethane / 3 h / -78 - 20 °C / Inert atmosphere

With pyrrolidine; methanol; triethylsilane; aluminum (III) chloride; sodium tetrahydroborate; diethylamino-sulfur trifluoride; isopropylmagnesium chloride; boron tribromide; sodium hydride; caesium carbonate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;