4-((3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenoxy)methyl)aniline

Base Information

Chemical Name:4-((3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenoxy)methyl)aniline
CAS No.:1278547-54-8
Molecular Formula:C₁₅H₁₁Cl₂F₄NO₂
Molecular Weight:384.157
Hs Code.:

Synonyms:4-((3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenoxy)methyl)aniline

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Chemical Property of 4-((3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenoxy)methyl)aniline

Chemical Property:

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Technology Process of 4-((3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenoxy)methyl)aniline

There total 4 articles about 4-((3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenoxy)methyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.5%

: 1278547-53-7
1,3-dichloro-5-(4-nitrobenzyloxy)-2-(1,1,2,2-tetrafluoroethoxy)benzene

: 1278547-54-8
4-((3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenoxy)methyl)aniline

Guidance literature:: With copper; ammonium chloride; zinc; In diethyl ether; water; at 25 ℃; for 5h;
DOI:10.1021/jf104578j

Reference yield:

: 3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenol

: 1278547-54-8
4-((3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenoxy)methyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol

1.2: 1 h / 25 °C

2.1: copper; ammonium chloride; zinc / diethyl ether; water / 5 h / 25 °C

With copper; ammonium chloride; sodium hydroxide; zinc; In diethyl ether; ethanol; water;
DOI:10.1021/jf104578j

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 1278547-54-8
4-((3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)-phenoxy)methyl)aniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol

1.2: 1 h / 25 °C

2.1: copper; ammonium chloride; zinc / diethyl ether; water / 5 h / 25 °C

With copper; ammonium chloride; sodium hydroxide; zinc; In diethyl ether; ethanol; water;
DOI:10.1021/jf104578j