(S)-2-Amino-pentanedioic acid diamide; compound with toluene-4-sulfonic acid

Base Information

Chemical Name:(S)-2-Amino-pentanedioic acid diamide; compound with toluene-4-sulfonic acid
CAS No.:86095-99-0
Molecular Formula:C₅H₁₁N₃O₂*C₇H₈O₃S
Molecular Weight:317.366
Hs Code.:

Synonyms:(S)-2-Amino-pentanedioic acid diamide; compound with toluene-4-sulfonic acid

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Chemical Property of (S)-2-Amino-pentanedioic acid diamide; compound with toluene-4-sulfonic acid

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Technology Process of (S)-2-Amino-pentanedioic acid diamide; compound with toluene-4-sulfonic acid

There total 2 articles about (S)-2-Amino-pentanedioic acid diamide; compound with toluene-4-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1155-62-0
N-benzyloxycarbonyl-L-glutamic acid

: 86095-99-0
(S)-2-Amino-pentanedioic acid diamide; compound with toluene-4-sulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) thionyl chloride; 2.) NH₃ / 1.) MeOH, 6 h, from 0 deg C to room temp; 2.) MeOH, -10 deg C, 30 min then room temp., 2 d

2: H₂ / 10percent Pd/C / dimethylformamide / 18 h

With thionyl chloride; ammonia; hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)97641-0

Reference yield:

: 76491-40-2,92043-67-9,2650-66-0
Cbz-L-Gln-NH₂

: 6192-52-5
p-toluenesulfonic acid monohydrate

: 86095-99-0
(S)-2-Amino-pentanedioic acid diamide; compound with toluene-4-sulfonic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide; for 18h; Yield given;
DOI:10.1016/S0040-4020(01)97641-0