O,O-dimethyl α(2-chloro-4-fluorophenoxyacetoxy)-2-hydroxybenzylphosphonate

Base Information

Chemical Name:O,O-dimethyl α(2-chloro-4-fluorophenoxyacetoxy)-2-hydroxybenzylphosphonate
CAS No.:1299293-64-3
Molecular Formula:C₁₇H₁₇ClFO₇P
Molecular Weight:418.743
Hs Code.:

Synonyms:O,O-dimethyl α(2-chloro-4-fluorophenoxyacetoxy)-2-hydroxybenzylphosphonate

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Chemical Property of O,O-dimethyl α(2-chloro-4-fluorophenoxyacetoxy)-2-hydroxybenzylphosphonate

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Technology Process of O,O-dimethyl α(2-chloro-4-fluorophenoxyacetoxy)-2-hydroxybenzylphosphonate

There total 3 articles about O,O-dimethyl α(2-chloro-4-fluorophenoxyacetoxy)-2-hydroxybenzylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: dimethyl α-hydroxy-2-hydroxybenzylphosphonate

: 826990-46-9
2-(2-chloro-4-fluorophenoxy)acetyl chloride

: 1299293-64-3
O,O-dimethyl α(2-chloro-4-fluorophenoxyacetoxy)-2-hydroxybenzylphosphonate

Guidance literature:: With triethylamine; In chloroform; at 2 - 20 ℃;
DOI:10.1021/jf104247w

Reference yield:

: 399-41-7
2-(2-chloro-4-fluorophenoxy)acetic acid

: 1299293-64-3
O,O-dimethyl α(2-chloro-4-fluorophenoxyacetoxy)-2-hydroxybenzylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride

2: triethylamine / chloroform / 2 - 20 °C

With thionyl chloride; triethylamine; In chloroform;
DOI:10.1021/jf104247w

Reference yield:

: 90-02-8
salicylaldehyde

: 1299293-64-3
O,O-dimethyl α(2-chloro-4-fluorophenoxyacetoxy)-2-hydroxybenzylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

2: triethylamine / chloroform / 2 - 20 °C

With triethylamine; In chloroform;
DOI:10.1021/jf104247w