N'-(2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbonyl)methanesulfonohydrazide

Base Information

Chemical Name:N'-(2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbonyl)methanesulfonohydrazide
CAS No.:1620951-96-3
Molecular Formula:C₂₄H₂₃N₅O₄S
Molecular Weight:477.544
Hs Code.:

Synonyms:N'-(2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbonyl)methanesulfonohydrazide

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Chemical Property of N'-(2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbonyl)methanesulfonohydrazide

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Technology Process of N'-(2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbonyl)methanesulfonohydrazide

There total 3 articles about N'-(2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbonyl)methanesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620955-57-8
C₁₆H₁₃BrN₄O₃S

: 1054480-13-5
2-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino)ethanol

: 1620951-96-3
N'-(2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbonyl)methanesulfonohydrazide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In 1,4-dioxane; ethanol; water; for 12h; Inert atmosphere; Reflux;

Reference yield:

: 1620955-56-7
C₁₅H₈BrClN₂O

: 1620951-96-3
N'-(2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbonyl)methanesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / ethanol; water; 1,4-dioxane / 12 h / Inert atmosphere; Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; water;

Reference yield:

: 121495-48-5
2-((4-iodophenyl)amino)ethanol

: 1620951-96-3
N'-(2-(4'-((2-hydroxyethyl)amino)-[1,1'-biphenyl]-4-yl)-1,6-naphthyridine-4-carbonyl)methanesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide / 14 h / 100 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / ethanol; water; 1,4-dioxane / 12 h / Inert atmosphere; Reflux

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; caesium carbonate; In 1,4-dioxane; ethanol; water; dimethyl sulfoxide;