(1R,2R,3S)-2-benzyloxy-3-(benzyloxymethyl)-1-(2-nitroethyl)-cyclopropyl 4-methylphenyl sulfone

Base Information

Chemical Name:(1R,2R,3S)-2-benzyloxy-3-(benzyloxymethyl)-1-(2-nitroethyl)-cyclopropyl 4-methylphenyl sulfone
CAS No.:1137932-09-2
Molecular Formula:C₂₇H₂₉NO₆S
Molecular Weight:495.596
Hs Code.:

Synonyms:(1R,2R,3S)-2-benzyloxy-3-(benzyloxymethyl)-1-(2-nitroethyl)-cyclopropyl 4-methylphenyl sulfone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,2R,3S)-2-benzyloxy-3-(benzyloxymethyl)-1-(2-nitroethyl)-cyclopropyl 4-methylphenyl sulfone

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Technology Process of (1R,2R,3S)-2-benzyloxy-3-(benzyloxymethyl)-1-(2-nitroethyl)-cyclopropyl 4-methylphenyl sulfone

There total 1 articles about (1R,2R,3S)-2-benzyloxy-3-(benzyloxymethyl)-1-(2-nitroethyl)-cyclopropyl 4-methylphenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 75-52-5
nitromethane

: 1137931-60-2
(2R,3R)-1,3-dibenzyloxy-4-[(4-methylphenyl)sulfonyl]pent-4-en-2-yl methanesulfonate

: 1137932-09-2
(1R,2R,3S)-2-benzyloxy-3-(benzyloxymethyl)-1-(2-nitroethyl)-cyclopropyl 4-methylphenyl sulfone

Guidance literature:: nitromethane; With sodium hydride; In N,N-dimethyl-formamide; Inert atmosphere;

(2R,3R)-1,3-dibenzyloxy-4-[(4-methylphenyl)sulfonyl]pent-4-en-2-yl methanesulfonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo802709q