C₃₃H₄₁NO₉Si

Base Information

Chemical Name:C₃₃H₄₁NO₉Si
CAS No.:1280608-62-9
Molecular Formula:C₃₃H₄₁NO₉Si
Molecular Weight:623.775
Hs Code.:

C<sub>33</sub>H<sub>41</sub>NO<sub>9</sub>Si

Synonyms:C₃₃H₄₁NO₉Si

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Chemical Property of C₃₃H₄₁NO₉Si

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Technology Process of C₃₃H₄₁NO₉Si

There total 9 articles about C₃₃H₄₁NO₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1280608-61-8
C₃₃H₄₃NO₉Si

: 1280608-62-9
C₃₃H₄₁NO₉Si

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-40-3
C₂₃H₂₅NO₆

: 1280608-62-9
C₃₃H₄₁NO₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

2.2: 2.5 h / 20 °C

3.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

4.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

5.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

6.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

7.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

8.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; Oxone; sodium tetrahydroborate; C₁₃H₂₀O₉; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; Dimethoxymethane; dichloromethane; water; acetonitrile; mineral oil; 3.1: Shi epoxidation / 8.1: Dess-Martin oxidation;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-50-5
C₂₃H₂₇NO₆

: 1280608-62-9
C₃₃H₄₁NO₉Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

1.2: 2.5 h / 20 °C

2.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

3.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

4.1: [bis(acetoxy)iodo]benzene; potassium hydroxide / 2 h / 0 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

6.1: pyridine; pyridine hydrofluoride / tetrahydrofuran / 8 h / -78 - 0 °C

7.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 - 20 °C

With pyridine; 2,6-dimethylpyridine; Oxone; C₁₃H₂₀O₉; pyridine hydrofluoride; [bis(acetoxy)iodo]benzene; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; Dimethoxymethane; dichloromethane; water; acetonitrile; mineral oil; 2.1: Shi epoxidation / 7.1: Dess-Martin oxidation;
DOI:10.1002/anie.201006528