Dithiocarbonic acid S-(1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl) ester O-(2,2-dimethyl-propyl) ester

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Chemical Name:Dithiocarbonic acid S-(1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl) ester O-(2,2-dimethyl-propyl) ester
CAS No.:181507-30-2
Molecular Formula:C₂₃H₃₃NO₅S₃
Molecular Weight:499.717
Hs Code.:

Synonyms:Dithiocarbonic acid S-(1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl) ester O-(2,2-dimethyl-propyl) ester

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Chemical Property of Dithiocarbonic acid S-(1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl) ester O-(2,2-dimethyl-propyl) ester

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Technology Process of Dithiocarbonic acid S-(1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl) ester O-(2,2-dimethyl-propyl) ester

There total 5 articles about Dithiocarbonic acid S-(1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl) ester O-(2,2-dimethyl-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: sodium O-neopentyl xanthate salt

: Methanesulfonic acid 1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl ester

: 181507-30-2
Dithiocarbonic acid S-(1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl) ester O-(2,2-dimethyl-propyl) ester

Guidance literature:: In acetone;
DOI:10.1016/0040-4039(96)01146-X

Reference yield:

: 59717-69-0
N-(2,2-diethoxyethyl)prop-2-en-1-amine

: 181507-30-2
Dithiocarbonic acid S-(1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl) ester O-(2,2-dimethyl-propyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1: NaOH / diethyl ether

2: CF₃CO₂H / H₂O; CHCl₃ / 0 °C

3: BuLi / tetrahydrofuran / -78 °C

5: 72 percent / acetone

With sodium hydroxide; n-butyllithium; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; chloroform; water; acetone;
DOI:10.1016/0040-4039(96)01146-X

Reference yield:

: 361459-74-7
4-methyl-N-(2-oxoethyl)-N-2-propen-1-ylbenzenesulfonamide

: 181507-30-2
Dithiocarbonic acid S-(1-{[allyl-(toluene-4-sulfonyl)-amino]-methyl}-4-methoxymethoxy-but-2-ynyl) ester O-(2,2-dimethyl-propyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: BuLi / tetrahydrofuran / -78 °C

3: 72 percent / acetone

With n-butyllithium; In tetrahydrofuran; acetone;
DOI:10.1016/0040-4039(96)01146-X