β,β-bis(o-methoxyphenyl)-α-methylvinyl bromide

Base Information

Chemical Name:β,β-bis(o-methoxyphenyl)-α-methylvinyl bromide
CAS No.:79517-72-9
Molecular Formula:C₁₇H₁₇BrO₂
Molecular Weight:333.225
Hs Code.:

Synonyms:β,β-bis(o-methoxyphenyl)-α-methylvinyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β,β-bis(o-methoxyphenyl)-α-methylvinyl bromide

Chemical Property:

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Technology Process of β,β-bis(o-methoxyphenyl)-α-methylvinyl bromide

There total 4 articles about β,β-bis(o-methoxyphenyl)-α-methylvinyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79517-75-2
1,1-bis(o-methoxyphenyl)propene

: 79517-72-9
β,β-bis(o-methoxyphenyl)-α-methylvinyl bromide

Guidance literature:: With bromine; In tetrachloromethane;
DOI:10.1021/jo00339a012

Reference yield:

: 16750-63-3
2-methoxyphenylmagnesium bromide

: 79517-72-9
β,β-bis(o-methoxyphenyl)-α-methylvinyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran / 0 - 20 °C

1.2: Reflux; Dean-Stark

2.1: bromine / 1,2-dichloro-ethane / 0.5 h / 0 °C

2.2: Reflux

With bromine; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/acscatal.6b01320

Reference yield:

: 578-57-4
2-bromoanisole

: 79517-72-9
β,β-bis(o-methoxyphenyl)-α-methylvinyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg / 1.) Et₂O

2: 85percent H₃PO₄ / 1.5 h / Heating

3: Br₂ / CCl₄

With phosphoric acid; bromine; magnesium; In tetrachloromethane;
DOI:10.1021/jo00339a012