C₃₁H₄₂N₂O₄*ClH

Base Information

Chemical Name:C₃₁H₄₂N₂O₄*ClH
CAS No.:1561903-30-7
Molecular Formula:C₃₁H₄₂N₂O₄*ClH
Molecular Weight:543.146
Hs Code.:

C<sub>31</sub>H<sub>42</sub>N<sub>2</sub>O<sub>4</sub>*ClH

Synonyms:C₃₁H₄₂N₂O₄*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₄₂N₂O₄*ClH

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Technology Process of C₃₁H₄₂N₂O₄*ClH

There total 7 articles about C₃₁H₄₂N₂O₄*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1561903-45-4
C₃₃H₄₆N₂O₄*ClH

: 1561903-30-7
C₃₁H₄₂N₂O₄*ClH

Guidance literature:: C₃₃H₄₆N₂O₄*ClH; With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; In methanol; diethyl ether; dichloromethane;
DOI:10.1039/c3ob42309c

Reference yield:

: 295-03-4
azacyclotridecane

: 1561903-30-7
C₃₁H₄₂N₂O₄*ClH

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

3.1: sodium iodide / tetrahydrofuran / 0.42 h / 20 °C / Inert atmosphere

3.2: 1 h / 20 °C

4.1: methanol / 0.5 h

4.2: 16 h / 45 °C

5.1: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

6.1: boron tribromide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; boron tribromide; triethylamine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide; pentane;
DOI:10.1039/c3ob42309c

Reference yield:

: 947-04-6,25038-74-8
2-azacyclotridecanone

: 1561903-30-7
C₃₁H₄₂N₂O₄*ClH

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere; Reflux

2.1: triethylamine / N,N-dimethyl-formamide / 16 h / 70 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / diethyl ether / 0.25 h / 0 - 33 °C / Inert atmosphere

4.1: sodium iodide / tetrahydrofuran / 0.42 h / 20 °C / Inert atmosphere

4.2: 1 h / 20 °C

5.1: methanol / 0.5 h

5.2: 16 h / 45 °C

6.1: hydrogenchloride / methanol; diethyl ether; chloroform; pentane

7.1: boron tribromide / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; boron tribromide; triethylamine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide; pentane;
DOI:10.1039/c3ob42309c