C₄₁H₆₆O₆Si₂

Base Information

Chemical Name:C₄₁H₆₆O₆Si₂
CAS No.:1416356-33-6
Molecular Formula:C₄₁H₆₆O₆Si₂
Molecular Weight:711.142
Hs Code.:

C<sub>41</sub>H<sub>66</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₄₁H₆₆O₆Si₂

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Chemical Property of C₄₁H₆₆O₆Si₂

Chemical Property:

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Technology Process of C₄₁H₆₆O₆Si₂

There total 21 articles about C₄₁H₆₆O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1416356-16-5
(1R,3R)-1-[(2R,3S,6R)-6-(Benzyloxymethyl)-5-methylene-3-(triethylsilyloxy)tetrahydropyran-2-yl]-5-(p-methoxybenzyloxy)-3-methyl-2-methylenepentan-1-ol

: 69739-34-0
t-butyldimethylsiyl triflate

: 1416356-33-6
C₄₁H₆₆O₆Si₂

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 - 20 ℃; for 1h;
DOI:10.1246/bcsj.20120152

Reference yield:

: 1416356-29-0
C₂₇H₄₈O₄Si₂

: 1416356-33-6
C₄₁H₆₆O₆Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: pyridinium p-toluenesulfonate / dichloromethane; methanol / 0.17 h / -10 °C

2: triethylamine; sulfur trioxide pyridine complex; dimethyl sulfoxide / dichloromethane / 0.5 h / 0 °C

3: sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogenphosphate / water; tert-butyl alcohol / 2 h / 0 - 20 °C

4: dicyclohexyl-carbodiimide; dmap / dichloromethane / 16 h / 0 - 20 °C

5: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; ((diphenylphosphoryl)oxy)copper(I); triphenyl-arsane / tetrahydrofuran / 3 h / 20 °C

6: zinc(II) tetrahydroborate / diethyl ether / 7.5 h / -40 °C

7: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

With 2,6-dimethylpyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium chlorite; sodium dihydrogenphosphate; zinc(II) tetrahydroborate; 2-methyl-but-2-ene; ((diphenylphosphoryl)oxy)copper(I); triphenyl-arsane; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; tert-butyl alcohol; 2: |Parikh-Doering Oxidation;
DOI:10.1246/bcsj.20120152

Reference yield:

: 315203-85-1
(2R,4aR,6S,7R,8aS)-2-Phenyl-6-vinyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-ol

: 1416356-33-6
C₄₁H₆₆O₆Si₂

Guidance literature:: Multi-step reaction with 15 steps

1.1: ozone / dichloromethane; methanol / -78 °C

1.2: -78 - 0 °C

2.1: 1H-imidazole / tetrahydrofuran; dichloromethane / 0 - 20 °C

3.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 20 °C / Molecular sieve

4.1: n-butyllithium / tetrahydrofuran / 0 - 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

6.1: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C

7.1: camphor-10-sulfonic acid / dichloromethane; methanol / 20 °C

8.1: 1H-imidazole / N,N-dimethyl-formamide / 61.5 h / 50 °C

9.1: pyridinium p-toluenesulfonate / dichloromethane; methanol / 0.17 h / -10 °C

10.1: triethylamine; sulfur trioxide pyridine complex; dimethyl sulfoxide / dichloromethane / 0.5 h / 0 °C

11.1: sodium chlorite; 2-methyl-but-2-ene; sodium dihydrogenphosphate / water; tert-butyl alcohol / 2 h / 0 - 20 °C

12.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 16 h / 0 - 20 °C

13.1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; ((diphenylphosphoryl)oxy)copper(I); triphenyl-arsane / tetrahydrofuran / 3 h / 20 °C

14.1: zinc(II) tetrahydroborate / diethyl ether / 7.5 h / -40 °C

15.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 0 - 20 °C

With 1H-imidazole; 2,6-dimethylpyridine; dmap; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; tetrapropylammonium perruthennate; zinc(II) tetrahydroborate; 2-methyl-but-2-ene; ((diphenylphosphoryl)oxy)copper(I); triphenyl-arsane; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; pyridinium p-toluenesulfonate; sodium hydride; ozone; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 10.1: |Parikh-Doering Oxidation;
DOI:10.1246/bcsj.20120152