Technology Process of 1-isothiocyanato-4-(phenylsulfonyl)benzene
There total 6 articles about 1-isothiocyanato-4-(phenylsulfonyl)benzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / Reflux
2: potassium carbonate; copper diacetate; oxygen / dimethyl sulfoxide / 45 °C / Molecular sieve
3: iron; acetic acid / 2 h / 60 °C
4: sodium hydrogencarbonate / water; chloroform / 2 h / 20 °C / Inert atmosphere
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; oxygen; potassium acetate; copper diacetate; iron; sodium hydrogencarbonate; potassium carbonate; acetic acid;
In
1,4-dioxane; chloroform; water; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; copper diacetate; oxygen / dimethyl sulfoxide / 45 °C / Molecular sieve
2: iron; acetic acid / 2 h / 60 °C
3: sodium hydrogencarbonate / water; chloroform / 2 h / 20 °C / Inert atmosphere
With
oxygen; copper diacetate; iron; sodium hydrogencarbonate; potassium carbonate; acetic acid;
In
chloroform; water; dimethyl sulfoxide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: iron; acetic acid / 2 h / 60 °C
2: sodium hydrogencarbonate / water; chloroform / 2 h / 20 °C / Inert atmosphere
With
iron; sodium hydrogencarbonate; acetic acid;
In
chloroform; water;
