N-(4-chlorobenzylidene)-2,6-diisopropylbenzeneamine

Base Information

Chemical Name:N-(4-chlorobenzylidene)-2,6-diisopropylbenzeneamine
CAS No.:117696-84-1
Molecular Formula:C₁₉H₂₂ClN
Molecular Weight:299.843
Hs Code.:

Synonyms:N-(4-chlorobenzylidene)-2,6-diisopropylbenzeneamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-chlorobenzylidene)-2,6-diisopropylbenzeneamine

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Technology Process of N-(4-chlorobenzylidene)-2,6-diisopropylbenzeneamine

There total 1 articles about N-(4-chlorobenzylidene)-2,6-diisopropylbenzeneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 24544-04-5
2,6-diisopropylbenzenamine

: 104-88-1
4-chlorobenzaldehyde

: 117696-84-1
N-(4-chlorobenzylidene)-2,6-diisopropylbenzeneamine

Guidance literature:: With 5% sulfaneted anatase-titania (TiO₂-SO₄^-2); In neat (no solvent); at 20 ℃; for 0.333333h; Catalytic behavior; Milling;

Reference yield: 75.0%

: 117696-84-1
N-(4-chlorobenzylidene)-2,6-diisopropylbenzeneamine

: palladium dichloride

: 710294-18-1
(PdCl(ClC₆H₃CHNC₆H₃(CH(CH₃)2)2))2

Guidance literature:: With sodium acetate; In tetrahydrofuran; under N2; pre-dried MeCN added to PdCl2; stirred at room temp. for 2 d; solvent removed to dryness; ligand (1.06 equiv.), Na acetate (15.5 equiv.) and THF added; stirred at room temp. for 38 h; solvent removed; CH2Cl2 added; filtered through Celite; filtrate concd.;washed with hexane; elem. anal.;
DOI:10.1016/j.jorganchem.2004.03.002