9-{2-[((1R,2S)-1-tert-butoxycarbonylamino-2-vinyl-cyclopropanecarbonyl)-sulfamoyl]-phenylamino}-nonanoic acid methyl ester

Base Information

Chemical Name:9-{2-[((1R,2S)-1-tert-butoxycarbonylamino-2-vinyl-cyclopropanecarbonyl)-sulfamoyl]-phenylamino}-nonanoic acid methyl ester
CAS No.:1051391-83-3
Molecular Formula:C₂₇H₄₁N₃O₇S
Molecular Weight:551.704
Hs Code.:

Synonyms:9-{2-[((1R,2S)-1-tert-butoxycarbonylamino-2-vinyl-cyclopropanecarbonyl)-sulfamoyl]-phenylamino}-nonanoic acid methyl ester

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Chemical Property of 9-{2-[((1R,2S)-1-tert-butoxycarbonylamino-2-vinyl-cyclopropanecarbonyl)-sulfamoyl]-phenylamino}-nonanoic acid methyl ester

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Technology Process of 9-{2-[((1R,2S)-1-tert-butoxycarbonylamino-2-vinyl-cyclopropanecarbonyl)-sulfamoyl]-phenylamino}-nonanoic acid methyl ester

There total 5 articles about 9-{2-[((1R,2S)-1-tert-butoxycarbonylamino-2-vinyl-cyclopropanecarbonyl)-sulfamoyl]-phenylamino}-nonanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1931-63-1
methyl ester of azelaic acid aldehyde

: 954271-75-1
[(1R,2S)-1-(2-amino-benzenesulfonylaminocarbonyl)-2-vinyl-cyclopropyl]-carbamic acid tert-butyl ester

: 1051391-83-3
9-{2-[((1R,2S)-1-tert-butoxycarbonylamino-2-vinyl-cyclopropanecarbonyl)-sulfamoyl]-phenylamino}-nonanoic acid methyl ester

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 15h;

Reference yield:

: 159622-10-3,213316-50-8,259221-77-7
(1R,2S)-1-(tert-butoxycarbonylamino)-2-vinylcyclopropanecarboxylic acid

: 1051391-83-3
9-{2-[((1R,2S)-1-tert-butoxycarbonylamino-2-vinyl-cyclopropanecarbonyl)-sulfamoyl]-phenylamino}-nonanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 1 - 2 h / Heating / reflux

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.75 h / 20 °C

3: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 15 h / 20 °C

With sodium tris(acetoxy)borohydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; 1,2-dichloro-ethane;

Reference yield:

: C₁₄H₁₉N₃O₃

: 1051391-83-3
9-{2-[((1R,2S)-1-tert-butoxycarbonylamino-2-vinyl-cyclopropanecarbonyl)-sulfamoyl]-phenylamino}-nonanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.75 h / 20 °C

2: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 15 h / 20 °C

With sodium tris(acetoxy)borohydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; 1,2-dichloro-ethane;