erythro-5,6-bis(4-hydroxyphenyl)-1-triethylene glycol monooctyl ether

Base Information

Chemical Name:erythro-5,6-bis(4-hydroxyphenyl)-1-triethylene glycol monooctyl ether
CAS No.:120579-10-4
Molecular Formula:C₂₆H₃₈O₆
Molecular Weight:446.584
Hs Code.:

Synonyms:erythro-5,6-bis(4-hydroxyphenyl)-1-triethylene glycol monooctyl ether

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Chemical Property of erythro-5,6-bis(4-hydroxyphenyl)-1-triethylene glycol monooctyl ether

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Technology Process of erythro-5,6-bis(4-hydroxyphenyl)-1-triethylene glycol monooctyl ether

There total 7 articles about erythro-5,6-bis(4-hydroxyphenyl)-1-triethylene glycol monooctyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 120579-01-3
erythro-5,6-bis<4-(benzyloxy)phenyl>-1-octyl triethylene glycol monoether

: 120579-10-4
erythro-5,6-bis(4-hydroxyphenyl)-1-triethylene glycol monooctyl ether

Guidance literature:: With hydrogen; palladium on activated charcoal; In cyclohexane; for 4h;
DOI:10.1021/jm00127a023

Reference yield:

: 107036-39-5,120578-90-7
(5S*,6R*)-5,6-bis(4-hydroxyphenyl)octanoic acid

: 120579-10-4
erythro-5,6-bis(4-hydroxyphenyl)-1-triethylene glycol monooctyl ether

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / potassium tert-butoxide / tetrahydrofuran / 4 h / Heating

2: 99 percent / lithium aluminum hydride / tetrahydrofuran / 4 h / Ambient temperature

3: 88 percent / N-methyl-N,N'-dicyclohexylcarbodiimidium iodide / tetrahydrofuran / Ambient temperature

4: 1) sodium hydride / 1) THF, 20 deg C, 0.5 h

5: 91 percent / H₂ / Pd/C / cyclohexane / 4 h

With lithium aluminium tetrahydride; potassium tert-butylate; hydrogen; sodium hydride; N,N'-dicyclohexyl-N-methylcarbodiimidium iodide; palladium on activated charcoal; In tetrahydrofuran; cyclohexane;
DOI:10.1021/jm00127a023

Reference yield:

: 107036-38-4,120578-47-4,120578-48-5
(5S*,6R*)-5,6-bis(4-methoxyphenyl)-1-octanoic acid

: 120579-10-4
erythro-5,6-bis(4-hydroxyphenyl)-1-triethylene glycol monooctyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / BBr₃ / CH₂Cl₂ / 3.5 h / Ambient temperature

2: 97 percent / potassium tert-butoxide / tetrahydrofuran / 4 h / Heating

3: 99 percent / lithium aluminum hydride / tetrahydrofuran / 4 h / Ambient temperature

4: 88 percent / N-methyl-N,N'-dicyclohexylcarbodiimidium iodide / tetrahydrofuran / Ambient temperature

5: 1) sodium hydride / 1) THF, 20 deg C, 0.5 h

6: 91 percent / H₂ / Pd/C / cyclohexane / 4 h

With lithium aluminium tetrahydride; potassium tert-butylate; hydrogen; boron tribromide; sodium hydride; N,N'-dicyclohexyl-N-methylcarbodiimidium iodide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; cyclohexane;
DOI:10.1021/jm00127a023