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C64H78N12O11

Base Information
  • Chemical Name:C64H78N12O11
  • CAS No.:1581698-79-4
  • Molecular Formula:C64H78N12O11
  • Molecular Weight:1191.4
  • Hs Code.:
C<sub>64</sub>H<sub>78</sub>N<sub>12</sub>O<sub>11</sub>

Synonyms:C64H78N12O11

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Chemical Property of C64H78N12O11
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Technology Process of C64H78N12O11

There total 5 articles about C64H78N12O11 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With triethylphosphite copper(I) iodide complex; In methanol; chloroform; at 100 ℃; for 3h; Reagent/catalyst; Temperature; Time; Sealed tube; Microwave irradiation;
DOI:10.1021/bc500047r
Guidance literature:
Multi-step reaction with 2 steps
1: hydrogen azide; triphenylphosphine; di-isopropyl azodicarboxylate / toluene; N,N-dimethyl-formamide / 0 - 20 °C
2: triethylphosphite copper(I) iodide complex / methanol; chloroform / 3 h / 100 °C / Sealed tube; Microwave irradiation
With hydrogen azide; triethylphosphite copper(I) iodide complex; di-isopropyl azodicarboxylate; triphenylphosphine; In methanol; chloroform; N,N-dimethyl-formamide; toluene; 2: |Huisgen Cycloaddition;
DOI:10.1021/bc500047r
Guidance literature:
Multi-step reaction with 4 steps
1: sodium hydride / toluene; N,N-dimethyl-formamide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere
2: trichlorophosphate / 12 h / 0 - 40 °C / Inert atmosphere
3: piperidine / acetonitrile / 12 h / 20 °C / Inert atmosphere
4: triethylphosphite copper(I) iodide complex / methanol; chloroform / 3 h / 100 °C / Sealed tube; Microwave irradiation
With piperidine; triethylphosphite copper(I) iodide complex; sodium hydride; trichlorophosphate; In methanol; chloroform; N,N-dimethyl-formamide; toluene; acetonitrile; mineral oil; 2: |Vilsmeier-Haack Formylation / 3: |Knoevenagel Condensation / 4: |Huisgen Cycloaddition;
DOI:10.1021/bc500047r
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