5-oxo-5-<<4-<2-oxo-2-<(1-phenylethyl)amino>ethyl>phenyl>amino>pentanoic acid

Base Information

Chemical Name:5-oxo-5-<<4-<2-oxo-2-<(1-phenylethyl)amino>ethyl>phenyl>amino>pentanoic acid
CAS No.:130468-90-5
Molecular Formula:C₂₁H₂₄N₂O₄
Molecular Weight:368.433
Hs Code.:

Synonyms:5-oxo-5-<<4-<2-oxo-2-<(1-phenylethyl)amino>ethyl>phenyl>amino>pentanoic acid

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Chemical Property of 5-oxo-5-<<4-<2-oxo-2-<(1-phenylethyl)amino>ethyl>phenyl>amino>pentanoic acid

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Technology Process of 5-oxo-5-<<4-<2-oxo-2-<(1-phenylethyl)amino>ethyl>phenyl>amino>pentanoic acid

There total 5 articles about 5-oxo-5-<<4-<2-oxo-2-<(1-phenylethyl)amino>ethyl>phenyl>amino>pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 108-55-4
glutaric anhydride,

: 31733-60-5
2-(4-aminophenyl)-N-(1-phenylethyl)acetamide

: 130468-90-5
5-oxo-5-<<4-<2-oxo-2-<(1-phenylethyl)amino>ethyl>phenyl>amino>pentanoic acid

Guidance literature:: With triethylamine; In dichloromethane; at 50 ℃; for 3.5h;
DOI:10.1021/ja00001a042

Reference yield:

: 1197-55-3
4-aminophenylacetic acid

: 130468-90-5
5-oxo-5-<<4-<2-oxo-2-<(1-phenylethyl)amino>ethyl>phenyl>amino>pentanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / sodium carbonate, water / acetonitrile / 0.17 h / 0 °C

2: 98 percent / thionyl chloride / 5 h / 55 °C

3: 57 percent / triethylamine / CH₂Cl₂ / 15 h / Ambient temperature

4: 55 percent / sodium borohydride / ethanol / 20 h / Ambient temperature

5: 30 percent / triethylamine / CH₂Cl₂ / 3.5 h / 50 °C

With sodium tetrahydroborate; thionyl chloride; water; sodium carbonate; triethylamine; In ethanol; dichloromethane; acetonitrile;
DOI:10.1021/ja00001a042

Reference yield:

: 113180-63-5
4-<(trifluoroacetyl)amino>benzeneacetyl chloride

: 130468-90-5
5-oxo-5-<<4-<2-oxo-2-<(1-phenylethyl)amino>ethyl>phenyl>amino>pentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / triethylamine / CH₂Cl₂ / 15 h / Ambient temperature

2: 55 percent / sodium borohydride / ethanol / 20 h / Ambient temperature

3: 30 percent / triethylamine / CH₂Cl₂ / 3.5 h / 50 °C

With sodium tetrahydroborate; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/ja00001a042