phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside
CAS No.:1322656-72-3
Molecular Formula:C₄₄H₅₉N₃O₂₂S
Molecular Weight:1014.03
Hs Code.:

phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

Synonyms:phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

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Chemical Property of phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₅₃N₃O₁₉S

: 108-24-7
acetic anhydride

: 1322656-72-3
phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: In pyridine; at 20 ℃; for 24h;
DOI:10.1016/j.carres.2011.03.029

Reference yield: 86.0%

: 1322656-72-3
phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

: 1322656-79-0
phenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

Guidance literature:: phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside; With sodium methylate; In methanol; at 20 ℃; for 24h; pH=8;

In methanol;
DOI:10.1016/j.carres.2011.03.029

Reference yield:

: 1322656-72-3
phenyl 3,4,6-tri-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-3,4-di-O-acetyl-2-acetamido-2-deoxy-1-thio-β-D-glucopyranoside

: 128960-84-9
N-((3R,4R,5S,6R)-4,5-dihydroxy-6-(hydroxymethyl)-2-(phenylthio)tetrahydro-2Hpyran-3-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / methanol / 24 h / 20 °C / pH 8

1.2: amberlite IR-120 (H+)

2.1: dispersin B; sodium chloride / water / 4 h / 25 °C / pH 5.9 / aq. phosphate buffer; Enzymatic reaction

3.1: dispersin B; sodium chloride / water / 4 h / 25 °C / pH 5.9 / aq. phosphate buffer; Enzymatic reaction

With dispersin B; sodium methylate; sodium chloride; In methanol; water;
DOI:10.1016/j.carres.2011.03.029